C₁₃H₁₈OSi

Base Information

Chemical Name:C₁₃H₁₈OSi
CAS No.:1310330-34-7
Molecular Formula:C₁₃H₁₈OSi
Molecular Weight:218.371
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₈OSi

Chemical Property:

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Technology Process of C₁₃H₁₈OSi

There total 3 articles about C₁₃H₁₈OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 7486-35-3
tri-n-butyl(vinyl)tin

: 151710-75-7
(Z)-3-(Dimethyl-phenyl-silanyl)-3-iodo-prop-2-en-1-ol

: 1310330-34-7
C₁₃H₁₈OSi

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); Tetrabutylammoniumsalz der Diphenylphosphinsaeure; In N,N-dimethyl-formamide; for 1h; Inert atmosphere;
DOI:10.1021/ja2031085

Reference yield:

: 43019-63-2
3-(phenyldimethylsilyl)prop-2-yn-1-ol

: 1310330-34-7
C₁₃H₁₈OSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether; toluene / 2 h / 20 °C / Inert atmosphere

1.2: 0.5 h / 20 °C / Inert atmosphere

2.1: dichloro bis(acetonitrile) palladium(II); Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 1 h / Inert atmosphere

With dichloro bis(acetonitrile) palladium(II); sodium bis(2-methoxyethoxy)aluminium dihydride; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; In diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja2031085

Reference yield:

: 862735-92-0
dimethyl(phenyl)(3-((tetrahydro-2H-pyran-2-yl)oxy)prop-1-yn-1-yl)silane

: 1310330-34-7
C₁₃H₁₈OSi

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol; toluene-4-sulfonic acid / 2 h / Inert atmosphere

2.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether; toluene / 2 h / 20 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

3.1: dichloro bis(acetonitrile) palladium(II); Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 1 h / Inert atmosphere

With methanol; dichloro bis(acetonitrile) palladium(II); toluene-4-sulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; In diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja2031085