2,4'-dihydroxy-2'-methoxycarbonyldiphenyl ether

Base Information

Chemical Name:2,4'-dihydroxy-2'-methoxycarbonyldiphenyl ether
CAS No.:77896-13-0
Molecular Formula:C₁₄H₁₂O₅
Molecular Weight:260.246
Hs Code.:

Synonyms:

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Chemical Property of 2,4'-dihydroxy-2'-methoxycarbonyldiphenyl ether

Chemical Property:

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Technology Process of 2,4'-dihydroxy-2'-methoxycarbonyldiphenyl ether

There total 5 articles about 2,4'-dihydroxy-2'-methoxycarbonyldiphenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27060-75-9
4-bromo-3-methylanisole

: 77896-13-0
2,4'-dihydroxy-2'-methoxycarbonyldiphenyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: copper, potassium carbonate / pyridine / 5 h / 170 °C

2: 5.0 g / potassium permanganate / pyridine; H₂O / 2 h / Heating

3: 6.2 g / pyridine hydrochloride / 2 h / 190 °C

4: acetyl chloride

With potassium permanganate; pyridine hydrochloride; copper; potassium carbonate; acetyl chloride; In pyridine; water;
DOI:10.1039/P19810000493

Reference yield:

: 77896-05-0
2,4'-dimethoxy-2'-methyldiphenyl ether

: 77896-13-0
2,4'-dihydroxy-2'-methoxycarbonyldiphenyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 5.0 g / potassium permanganate / pyridine; H₂O / 2 h / Heating

2: 6.2 g / pyridine hydrochloride / 2 h / 190 °C

3: acetyl chloride

With potassium permanganate; pyridine hydrochloride; acetyl chloride; In pyridine; water;
DOI:10.1039/P19810000493

Reference yield:

: 90-05-1
2-methoxy-phenol

: 77896-13-0
2,4'-dihydroxy-2'-methoxycarbonyldiphenyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: copper, potassium carbonate / pyridine / 5 h / 170 °C

2: 5.0 g / potassium permanganate / pyridine; H₂O / 2 h / Heating

3: 6.2 g / pyridine hydrochloride / 2 h / 190 °C

4: acetyl chloride

With potassium permanganate; pyridine hydrochloride; copper; potassium carbonate; acetyl chloride; In pyridine; water;
DOI:10.1039/P19810000493