Technology Process of C20H26N4O3S
There total 7 articles about C20H26N4O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane
2: hydrogenchloride / water; 1,4-dioxane
3: N-ethyl-N,N-diisopropylamine / dichloromethane
With
hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.01.104
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / water; 1,4-dioxane
2: N-ethyl-N,N-diisopropylamine / dichloromethane
With
hydrogenchloride; N-ethyl-N,N-diisopropylamine;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.01.104
- Guidance literature:
-
Multi-step reaction with 6 steps
1: triethylamine / dichloromethane
2: trichlorophosphate; 1H-imidazole; pyridine
3: hydrogenchloride / water; 1,4-dioxane; diethyl ether
4: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane
5: hydrogenchloride / water; 1,4-dioxane
6: N-ethyl-N,N-diisopropylamine / dichloromethane
With
pyridine; 1H-imidazole; hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; trichlorophosphate;
In
1,4-dioxane; diethyl ether; dichloromethane; water;
DOI:10.1016/j.bmcl.2013.01.104
