4'-hexyloxybiphenyl-4-yl 2-(((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-yl)-N-methylamino)acetate

Base Information

Chemical Name:4'-hexyloxybiphenyl-4-yl 2-(((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-yl)-N-methylamino)acetate
CAS No.:1400891-41-9
Molecular Formula:C₃₅H₄₆BrNO₆
Molecular Weight:656.657
Hs Code.:

4'-hexyloxybiphenyl-4-yl 2-(((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-yl)-N-methylamino)acetate

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Chemical Property of 4'-hexyloxybiphenyl-4-yl 2-(((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-yl)-N-methylamino)acetate

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Technology Process of 4'-hexyloxybiphenyl-4-yl 2-(((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-yl)-N-methylamino)acetate

There total 2 articles about 4'-hexyloxybiphenyl-4-yl 2-(((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-yl)-N-methylamino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1350562-65-0
C₁₇H₂₆BrNO₅

: 78435-17-3
4-hexyloxy-4'-hydroxybiphenyl

: 1400891-41-9
4'-hexyloxybiphenyl-4-yl 2-(((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-yl)-N-methylamino)acetate

Guidance literature:: C₁₇H₂₆BrNO₅; With dicyclohexyl-carbodiimide; In dichloromethane; for 0.5h; Reflux;

4-hexyloxy-4'-hydroxybiphenyl; With dmap; In dichloromethane; for 72h; Reflux;
DOI:10.1007/s11164-012-0777-5

Reference yield:

: 153179-99-8
C₁₄H₂₀Br₂O₃

: 1400891-41-9
4'-hexyloxybiphenyl-4-yl 2-(((S)-4-bromo-2-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyloxy)-5-oxo-2,5-dihydrofuran-3-yl)-N-methylamino)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol / 20 °C

2.1: dicyclohexyl-carbodiimide / dichloromethane / 0.5 h / Reflux

2.2: 72 h / Reflux

With dicyclohexyl-carbodiimide; potassium hydroxide; In ethanol; dichloromethane;
DOI:10.1007/s11164-012-0777-5