2-bromo-5,6-dichloro-1-β-D-ribofuranosylbenzimidazole

Base Information

Chemical Name:2-bromo-5,6-dichloro-1-β-D-ribofuranosylbenzimidazole
CAS No.:142356-43-2
Molecular Formula:C₁₂H₁₁BrCl₂N₂O₄
Molecular Weight:398.04
Hs Code.:

Synonyms:

Suppliers and Price of 2-bromo-5,6-dichloro-1-β-D-ribofuranosylbenzimidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-bromo-5,6-dichloro-1-β-D-ribofuranosylbenzimidazole

Chemical Property:

Purity/Quality:: 98% by HPLC ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-bromo-5,6-dichloro-1-β-D-ribofuranosylbenzimidazole

There total 7 articles about 2-bromo-5,6-dichloro-1-β-D-ribofuranosylbenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 142356-42-1
2-bromo-5,6-dichloro-1-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)benzimidazole

: 142356-43-2
2-bromo-5,6-dichloro-1-β-D-ribofuranosylbenzimidazole

Guidance literature:: With ammonia; for 16h; Ambient temperature;
DOI:10.1021/jm00020a025

Reference yield:

: 28708-32-9
1,2,3,5-tetra-O-acetyl-D-ribofuranose

: 142356-40-9
2-bromo-5,6-dichloro-1H-1,3-benzodiazole

: 13035-61-5
1,2,3,5-tetraacetylribose

: 142356-43-2
2-bromo-5,6-dichloro-1-β-D-ribofuranosylbenzimidazole

Guidance literature:: With benzenesulfonamide; In acetonitrile;

Reference yield:

: 5348-42-5
4,5-Dichloro-1,2-phenylenediamine

: 142356-43-2
2-bromo-5,6-dichloro-1-β-D-ribofuranosylbenzimidazole

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / methanol; H₂O; acetonitrile / Ambient temperature

2: 1.) aq. HBr, NaNO₂, 2.) CuBr / 1.) RT, 1 h, 2.) water, 100 deg C, 1 h

3: acetonitrile / 0.17 h / 60 °C

4: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 1 h / 60 °C

5: 37 percent / methanolic ammonia / 16 h / Ambient temperature

With trimethylsilyl trifluoromethanesulfonate; ammonia; hydrogen bromide; copper(I) bromide; sodium nitrite; In methanol; water; acetonitrile;
DOI:10.1021/jm00020a025