N,N'-bis(2-pyridylmethyl)-3,4-diamino-2,5-diphenylthiophene

Base Information

• Chemical Name: N,N'-bis(2-pyridylmethyl)-3,4-diamino-2,5-diphenylthiophene
• CAS No.: 1252652-42-8
• Molecular Formula: C₂₈H₂₄N₄S
• Molecular Weight: 448.591
• Mol file: 1252652-42-8.mol

Synonyms:

Chemical Property of N,N'-bis(2-pyridylmethyl)-3,4-diamino-2,5-diphenylthiophene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N,N'-bis(2-pyridylmethyl)-3,4-diamino-2,5-diphenylthiophene

There total 1 articles about N,N'-bis(2-pyridylmethyl)-3,4-diamino-2,5-diphenylthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C28H20N4S → N,N'-bis(2-pyridylmethyl)-3,4-diamino-2,5-diphenylthiophene (1252652-42-8)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 75 ℃; for 1h; Inert atmosphere;

DOI:10.1139/V10-086

Reference yield: 50.0%

iron(II) tetrafluoroborate hexahydrate + N,N'-bis(2-pyridylmethyl)-3,4-diamino-2,5-diphenylthiophene (1252652-42-8) + potassium thioacyanate (333-20-0) → [Fe(N,N'-bis(2-pyridylmethyl)-3,4-diamino-2,5-diphenylthiophene)(NCS)2]

Guidance literature:

In methanol; water; a soln. of thiophene-compound in methanol was degassed by sparging with N2 for 0.5 h, Fe-complex was added, the mixt. was stirred for 0.5 h under N2, KSCN in H2O was added; diethyl ether was added, ppt. was vac. filtered; elem. anal.;

DOI:10.1139/V10-086