C₂₂H₃₅N₃O₄

Base Information

• Chemical Name: C₂₂H₃₅N₃O₄
• CAS No.: 1265223-04-8
• Molecular Formula: C₂₂H₃₅N₃O₄
• Molecular Weight: 405.538
• Mol file: 1265223-04-8.mol

Synonyms:

Chemical Property of C₂₂H₃₅N₃O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₃₅N₃O₄

There total 3 articles about C₂₂H₃₅N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H33N3O3 → C22H35N3O4 (1265223-04-8)

Guidance literature:

Multi-step reaction with 3 steps

1: hydroxylamine; potassium carbonate / ethanol / Reflux

2: pyridine / 20 °C

3: sodium sulfate / 60 °C

With pyridine; hydroxylamine; potassium carbonate; sodium sulfate; In ethanol; 3: Neber rearrangement;

DOI:10.1016/j.bmcl.2012.02.073

Reference yield:

C25H31N3O5S (1373162-64-1) + potassium ethoxide (917-58-8) → C22H35N3O4 (1265223-04-8)

Guidance literature:

With sodium sulfate; at 60 ℃;

DOI:10.1016/j.bmcl.2012.02.073

Reference yield:

C18H25N3O3 (1373162-63-0) → C22H35N3O4 (1265223-04-8)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / 20 °C

2: sodium sulfate / 60 °C

With pyridine; sodium sulfate; 2: Neber rearrangement;

DOI:10.1016/j.bmcl.2012.02.073

upstream raw materials:

C₁₈H₂₅N₃O₃

C₂₅H₃₁N₃O₅S

potassium ethoxide

Downstream raw materials:

C₂₃H₃₀N₄O₄