diethylmethylammonio-N-diphenylphosphinoylimide

Base Information

Chemical Name:diethylmethylammonio-N-diphenylphosphinoylimide
CAS No.:124730-91-2
Molecular Formula:C₁₇H₂₃N₂OP
Molecular Weight:302.356
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethylmethylammonio-N-diphenylphosphinoylimide

Chemical Property:

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Technology Process of diethylmethylammonio-N-diphenylphosphinoylimide

There total 1 articles about diethylmethylammonio-N-diphenylphosphinoylimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88240-69-1
1,1-diethyl-2-diphenylphosphinoylhydrazine

: 74-88-4
methyl iodide

: 124730-91-2
diethylmethylammonio-N-diphenylphosphinoylimide

Guidance literature:: at 50 ℃; for 24h; Yield given; closed vessel;

Reference yield: 32.0%

: 124730-91-2
diethylmethylammonio-N-diphenylphosphinoylimide

: 74-88-4
methyl iodide

: 132509-14-9
1,1-diethyl-1,2-dimethyl-2-diphenylphosphinoylhydrazinium iodide

Guidance literature:: at 45 ℃; for 16h;

Reference yield:

: 124730-91-2
diethylmethylammonio-N-diphenylphosphinoylimide

: 25530-11-4
diphenylphosphinic acid N-methylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 32 percent / 16 h / 45 °C

2: t-BuOK / tetrahydrofuran / 0.17 h

3: CDCl₃ / decomposition

With potassium tert-butylate; In tetrahydrofuran; chloroform-d1;