C₁₇H₁₄F₃N₃OS

Base Information

Chemical Name:C₁₇H₁₄F₃N₃OS
CAS No.:827010-27-5
Molecular Formula:C₁₇H₁₄F₃N₃OS
Molecular Weight:365.379
Hs Code.:

C<sub>17</sub>H<sub>14</sub>F<sub>3</sub>N<sub>3</sub>OS

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₁₄F₃N₃OS

Chemical Property:

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Technology Process of C₁₇H₁₄F₃N₃OS

There total 4 articles about C₁₇H₁₄F₃N₃OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104960-49-8
2-thioxo-6-phenyl-4-(trifluoromethyl)-1,2-dihydropyridine-3-carbonitrile

: 827010-27-5
C₁₇H₁₄F₃N₃OS

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / N,N-dimethyl-formamide; water / 20 °C

2: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.01.075

Reference yield:

: 299165-10-9
ethyl 3-amino-6-phenyl-4-trifluoromethylthiophene[2,3-b]pyridine-2-ethyl ester

: 827010-27-5
C₁₇H₁₄F₃N₃OS

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2014.01.075

Reference yield:

: 98-86-2
acetophenone

: 827010-27-5
C₁₇H₁₄F₃N₃OS

Guidance literature:: Multi-step reaction with 5 steps

1: sodium methylate / methanol; tetrahydrofuran / 0 - 20 °C

2: 1,4-diaza-bicyclo[2.2.2]octane / ethanol / 20 °C / Reflux

3: potassium hydroxide / N,N-dimethyl-formamide; water / 20 °C

4: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; sodium methylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; potassium hydroxide; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.01.075