11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carboxylic acid methyl ester

Base Information

• Chemical Name: 11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carboxylic acid methyl ester
• CAS No.: 121843-15-0
• Molecular Formula: C₂₃H₃₀O₇
• Molecular Weight: 418.487

Synonyms:

Chemical Property of 11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carboxylic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carboxylic acid methyl ester

There total 2 articles about 11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carbonitrile + methanol (67-56-1) → 11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carboxylic acid methyl ester (121843-15-0)

Guidance literature:

11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carbonitrile; methanol; With hydrogenchloride; at -25 - 0 ℃;

With water; sodium carbonate; pH=3 - 4;

DOI:10.1080/00397910601038954

Reference yield:

11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carbonitrile + methanol (67-56-1) → 17-dimethoxyacetyl-11-hydroxy-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carboxylic acid methyl ester + 11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carboxylic acid methyl ester (121843-15-0) + 11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carboxylic acid amide

Guidance literature:

11,17-dihydroxy-17-hydroxyacetyl-10,13-dimethyl-3-oxo-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-3H-cyclopenta[a]phenanthrene-16-carbonitrile; methanol; With hydrogenchloride; at -25 - -10 ℃;

With water; sodium carbonate; pH=3 - 4;

DOI:10.1080/00397910601038954

upstream raw materials:

methanol

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