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phenanthrenechromium dicarbonyl triphenylstibine

Base Information
  • Chemical Name:phenanthrenechromium dicarbonyl triphenylstibine
  • CAS No.:73656-14-1
  • Molecular Formula:C34H25CrO2Sb
  • Molecular Weight:639.317
  • Hs Code.:
phenanthrenechromium dicarbonyl triphenylstibine

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Chemical Property of phenanthrenechromium dicarbonyl triphenylstibine
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Technology Process of phenanthrenechromium dicarbonyl triphenylstibine

There total 1 articles about phenanthrenechromium dicarbonyl triphenylstibine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With C4H8O; In tetrahydrofuran; Irradiation (UV/VIS); (N2); soln. of Cr complex was UV irradiated until Cr-THF complex had formed, monitored by IR, then equimolar amt. of ligand was added and soln.was allowed to stand for 30 min at room temp.; soln. was evapd. under vac., residue dissolved in benzene/PE (1/1) and chromd. (silicagel, benzene/PE, first 1/1, increasing benzene content), last band yielded product; recrystn. from cyclohexane/PE;
DOI:10.1016/S0022-328X(00)94367-5
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