(C₆H₅)2HGeGe(CH₃)(C₆H₅)2

Base Information

• Chemical Name: (C₆H₅)2HGeGe(CH₃)(C₆H₅)2
• CAS No.: 151920-27-3
• Molecular Formula: C₂₅H₂₄Ge₂
• Molecular Weight: 469.646

Synonyms:

Chemical Property of (C₆H₅)2HGeGe(CH₃)(C₆H₅)2

Chemical Property:

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Technology Process of (C₆H₅)2HGeGe(CH₃)(C₆H₅)2

There total 2 articles about (C₆H₅)2HGeGe(CH₃)(C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1,2,2-tetraphenyl 1,2-digermane (13891-99-1) → (C6H5)2HGeGe(CH3)(C6H5)2 (151920-27-3) + diphenylgermylene (68816-03-5)

Guidance literature:

With water; tert.-butyl lithium; methyl iodide; In tetrahydrofuran; pentane; byproducts: (C6H5)2GeH2, LiI, (C6H5)2HGeCH3; under N2 Or Ar. addn. of a deficiency of t-BuLi in pentane to a soln. of the digermyl compd. in THF at -40°C, stirring for 30 min, -40°C, addn. of an excess of MeI, warming to ambient temp., 30 min at 20°C, hydrolysis; extn., concg. under vac., 1H NMR, not isolated;

DOI:10.1016/S0020-1693(00)92307-7

Reference yield:

1,1,2,2-tetraphenyl 1,2-digermane (13891-99-1) → (C6H5)2HGeGe(CH3)(C6H5)2 (151920-27-3) + 1,2-dimethyl-1,1,2,2-tetraphenylgermane (13892-12-1) + diphenylgermylene (68816-03-5)

Guidance literature:

With water; tert.-butyl lithium; methyl iodide; In tetrahydrofuran; pentane; byproducts: BuH, LiI; under N2 or Ar, addn. of t-BuLi in pentane to a soln. of the digermyl compd. in THF at -40°C, stirring for 30 min, -40°C, addn. of an excess of MeI, warming to ambient temp., 30 min at 20°C, hydrolysis; extn., concg. under vac., 1H NMR, not isolated;

DOI:10.1016/S0020-1693(00)92307-7

upstream raw materials:

1,1,2,2-tetraphenyl 1,2-digermane

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