(benzyloxycarbonyl)cobalt tetracarbonyl

Base Information

Chemical Name:(benzyloxycarbonyl)cobalt tetracarbonyl
CAS No.:97170-47-3
Molecular Formula:C₁₂H₇CoO₆
Molecular Weight:306.177
Hs Code.:

Synonyms:

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Chemical Property of (benzyloxycarbonyl)cobalt tetracarbonyl

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Technology Process of (benzyloxycarbonyl)cobalt tetracarbonyl

There total 1 articles about (benzyloxycarbonyl)cobalt tetracarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15976-97-3
tetracarbonyl iodo cobalt

: 45581-66-6
benzyl oxide ion

: 97170-47-3
(benzyloxycarbonyl)cobalt tetracarbonyl

Guidance literature:: With 12-crown-4 or 15-crown-5 or 18-crown-6; CO; In tetrahydrofuran; under CO, -78°C soln. of ICo(CO)4 in THF treated with Li, Na, orK alkoxide and 12-crown-4, 15-crown-5, or 18-crown-6, resp. during 3 h,stirred for addnl. 2 h, allowed to warm to 20-25°C; n-heptane added, filtered, evapd.;
DOI:10.1021/om00128a006

Reference yield:

: 97170-47-3
(benzyloxycarbonyl)cobalt tetracarbonyl

: 97170-63-3
C₆H₅CH₂OC(O)Co(CO)3P(C₆H₅)3

Guidance literature:: With PPh₃; In n-heptane; under Ar, soln. of educt in n-heptane treated with excess PPh3 at 20-25°C, stirred for 1 h; concd., filtered, crystd. at -78°C from Et2O/pentane, chromd. (n-hexane); elem. anal.;
DOI:10.1021/om00128a006

Reference yield:

: 97170-47-3
(benzyloxycarbonyl)cobalt tetracarbonyl

: 20194-18-7
sodium phenyl-methanolate

: 97170-75-7
[Co(COOCH₂C₆H₅)2(CO)3]^(1-)

Guidance literature:: With 15-crown-5; In tetrahydrofuran; n-heptane; under Ar, Co complex dissolved in n-heptane at 20-25°C, treated successively with THF, MeONa, and 15-crown-5, stirred for 20 min; not isolated; detected by IR;
DOI:10.1021/om00128a006