2,2,2-trifluoroethyl (Z)-O-methylbenzohydroximate

Base Information

• Chemical Name: 2,2,2-trifluoroethyl (Z)-O-methylbenzohydroximate
• CAS No.: 384338-19-6
• Molecular Formula: C₁₀H₁₀F₃NO₂
• Molecular Weight: 233.19
• Mol file: 384338-19-6.mol

Synonyms:

Chemical Property of 2,2,2-trifluoroethyl (Z)-O-methylbenzohydroximate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2,2-trifluoroethyl (Z)-O-methylbenzohydroximate

There total 2 articles about 2,2,2-trifluoroethyl (Z)-O-methylbenzohydroximate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-N-methoxybenzenecarboximidoyl chloride (41071-35-6) + sodium 2,2,2-trifluoroethanolate (420-87-1) → 2,2,2-trifluoroethyl (E)-O-methylbenzohydroximate (384338-15-2) + 2,2,2-trifluoroethyl (Z)-O-methylbenzohydroximate (384338-19-6)

Guidance literature:

(Z)-N-methoxybenzenecarboximidoyl chloride; sodium 2,2,2-trifluoroethanolate; In 2,2,2-trifluoroethanol; dimethyl sulfoxide; at 50 ℃; for 14h;

With acetic acid; at 80 ℃; for 3.5h; Further stages.;

DOI:10.1021/jo010067k

Reference yield:

2,2,2-trifluoroethyl (E)-O-methylbenzohydroximate (384338-15-2) → 2,2,2-trifluoroethyl (Z)-O-methylbenzohydroximate (384338-19-6)

Guidance literature:

In acetic acid; at 80 ℃; Equilibrium constant; Kinetics;

DOI:10.1021/jo010067k

upstream raw materials:

(Z)-N-methoxybenzenecarboximidoyl chloride

sodium 2,2,2-trifluoroethanolate

2,2,2-trifluoroethyl (E)-O-methylbenzohydroximate

Refernces