3--5-(trimethylsilyl)cyclohexanone

Base Information

Chemical Name:3--5-(trimethylsilyl)cyclohexanone
CAS No.:129156-37-2
Molecular Formula:C₁₄H₂₄O₅Si
Molecular Weight:300.427
Hs Code.:

3-<Bis(methoxycarbonyl)methyl>-5-(trimethylsilyl)cyclohexanone

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Suppliers and Price of 3--5-(trimethylsilyl)cyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3--5-(trimethylsilyl)cyclohexanone

Chemical Property:

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Technology Process of 3--5-(trimethylsilyl)cyclohexanone

There total 1 articles about 3--5-(trimethylsilyl)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 56917-71-6
5-trimethylsilyl-2-cyclohexanone

: 108-59-8
malonic acid dimethyl ester

: 129156-37-2,129156-48-5
3--5-(trimethylsilyl)cyclohexanone

Guidance literature:: With sodium methylate; In methanol; for 24h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81963-3

Reference yield:

: 129156-37-2,129156-48-5
3--5-(trimethylsilyl)cyclohexanone

: 129156-53-2
3-(2-hydroxyethyl)-5-(trimethylsilyl)cyclohexanone

Guidance literature:: Multi-step reaction with 3 steps

2: p-TosOH / methanol / 0.5 h / Ambient temperature

3: 1. LiAlH₄ 2. HCl / 1. THF, 0 deg C 2. H₂O

With hydrogenchloride; lithium aluminium tetrahydride; toluene-4-sulfonic acid; In methanol;
DOI:10.1016/S0040-4020(01)81963-3

Reference yield:

: 129156-37-2,129156-48-5
3--5-(trimethylsilyl)cyclohexanone

: ((1R,5R)-3,3-Dimethoxy-5-trimethylsilanyl-cyclohexyl)-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: p-TosOH / methanol / 0.5 h / Ambient temperature

With toluene-4-sulfonic acid; In methanol;
DOI:10.1016/S0040-4020(01)81963-3