cyclohomonervilol benzoate

Base Information

• Chemical Name: cyclohomonervilol benzoate
• CAS No.: 98155-95-4
• Molecular Formula: C₃₉H₅₈O₂
• Molecular Weight: 558.888
• Mol file: 98155-95-4.mol

Synonyms:

Chemical Property of cyclohomonervilol benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyclohomonervilol benzoate

There total 1 articles about cyclohomonervilol benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoyl chloride (98-88-4) + cyclohomonervilol (78330-51-5) → cyclohomonervilol benzoate (98155-95-4)

Guidance literature:

With pyridine; Ambient temperature;

Reference yield:

cyclohomonervilol benzoate (98155-95-4) → 24S-dihydrocyclofuntumienol benzoate (98155-98-7,98302-98-8,98303-02-7)

Guidance literature:

Multi-step reaction with 5 steps

1: 5.5 mg / osmium tetroxide / Ambient temperature

2: 1) HIO₄, 2) NaBH₄ / 1) dioxane-water, 8 min, ice-cooling; 2) MeOH, 30 min

3: 3.5 mg / pyridine / 12 h / Ambient temperature

4: 0.01 mg / tributyltin hydride / toluene / 4 h / 130 °C

5: H₂/PtO₂

With platinum(IV) oxide; sodium tetrahydroborate; osmium(VIII) oxide; hydrogen; tri-n-butyl-tin hydride; periodic acid; In pyridine; toluene;

Reference yield:

cyclohomonervilol benzoate (98155-95-4) → cyclofuntumienol benzoate (112515-96-5)

Guidance literature:

Multi-step reaction with 4 steps

1: 5.5 mg / osmium tetroxide / Ambient temperature

2: 1) HIO₄, 2) NaBH₄ / 1) dioxane-water, 8 min, ice-cooling; 2) MeOH, 30 min

3: 3.5 mg / pyridine / 12 h / Ambient temperature

4: 0.01 mg / tributyltin hydride / toluene / 4 h / 130 °C

With sodium tetrahydroborate; osmium(VIII) oxide; tri-n-butyl-tin hydride; periodic acid; In pyridine; toluene;

upstream raw materials:

benzoyl chloride

cyclohomonervilol

Downstream raw materials:

Benzoic acid (3S,4S,5S,9S,10R,13R,14S)-17-((1R,4S)-5,6-dihydroxy-4-isopropyl-1,5-dimethyl-hexyl)-4,13,14-trimethyl-tetradecahydro-cyclopropa[9,10]cyclopenta[a]phenanthren-3-yl ester

cyclofuntumienol benzoate

24S-dihydrocyclofuntumienol benzoate

Benzoic acid (3S,4S,5S,8S,9S,10R,13R,14S)-17-((1R,4R)-5,6-dihydroxy-4-isopropyl-1,5-dimethyl-hexyl)-4,13,14-trimethyl-tetradecahydro-cyclopropa[9,10]cyclopenta[a]phenanthren-3-yl ester