Technology Process of C28H30Cl4N4O14P2
There total 5 articles about C28H30Cl4N4O14P2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 89 percent / 1-(mesitylenesulphonyl)-3-nitro-1,2,4-triazole, pyridine / 1 h / Ambient temperature
2: 20percent trichloroacetic acid / CHCl3 / Ambient temperature
3: Et3N / acetonitrile / 1 h / Ambient temperature
4: pyridine, 1-(mesitylenesulphonyl)-3-nitro-1,2,4-triazole / 12 h / Ambient temperature
With
pyridine; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; triethylamine; trichloroacetic acid;
In
chloroform; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 89 percent / 1-(mesitylenesulphonyl)-3-nitro-1,2,4-triazole, pyridine / 1 h / Ambient temperature
2: 20percent trichloroacetic acid / CHCl3 / Ambient temperature
3: Et3N / acetonitrile / 1 h / Ambient temperature
4: pyridine, 1-(mesitylenesulphonyl)-3-nitro-1,2,4-triazole / 12 h / Ambient temperature
With
pyridine; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; triethylamine; trichloroacetic acid;
In
chloroform; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 20percent trichloroacetic acid / CHCl3 / Ambient temperature
2: Et3N / acetonitrile / 1 h / Ambient temperature
3: pyridine, 1-(mesitylenesulphonyl)-3-nitro-1,2,4-triazole / 12 h / Ambient temperature
With
pyridine; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; triethylamine; trichloroacetic acid;
In
chloroform; acetonitrile;