1--3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-(2-methoxycarbonylethyl)-2-nitropropane

Base Information

Chemical Name:1--3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-(2-methoxycarbonylethyl)-2-nitropropane
CAS No.:101210-42-8
Molecular Formula:C₄₂H₅₃N₃O₁₆
Molecular Weight:855.893
Hs Code.:

1-<Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-(2-methoxycarbonylethyl)-2-nitropropane

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Chemical Property of 1--3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-(2-methoxycarbonylethyl)-2-nitropropane

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Technology Process of 1--3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-(2-methoxycarbonylethyl)-2-nitropropane

There total 6 articles about 1--3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-(2-methoxycarbonylethyl)-2-nitropropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 101231-96-3
1-3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropane

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 101210-42-8
1--3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-(2-methoxycarbonylethyl)-2-nitropropane

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; In N,N-dimethyl-formamide; for 0.666667h; Ambient temperature;

Reference yield:

: 101210-40-6,101210-41-7
(E)- and (Z)-3-<5-Benzyloxycarbonyl-3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethylpyrrol-2-yl>-1-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-nitropropene

: 101210-42-8
1--3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-(2-methoxycarbonylethyl)-2-nitropropane

Guidance literature:: Multi-step reaction with 2 steps

1: borohydride

2: 1.) Triton B

With borohydride; N-benzyl-trimethylammonium hydroxide;
DOI:10.1039/c39850001294

Reference yield:

: 101210-39-3
Benzyl 4-(2-Methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-(2-nitroethyl)pyrrole-2-carboxylate

: 101210-42-8
1--3-<4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethyl-5-t-butoxycarbonylpyrrol-2-yl>-2-(2-methoxycarbonylethyl)-2-nitropropane

Guidance literature:: Multi-step reaction with 3 steps

1: methylamine / acetic acid

2: borohydride

3: 1.) Triton B

With borohydride; N-benzyl-trimethylammonium hydroxide; methylamine; In acetic acid;
DOI:10.1039/c39850001294