1-phenyl-2-fluoro-1,2-dicarba-closo-dodecaborane

Base Information

Chemical Name:1-phenyl-2-fluoro-1,2-dicarba-closo-dodecaborane
CAS No.:778595-92-9
Molecular Formula:C₈H₁₅B₁₀F
Molecular Weight:238.316
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenyl-2-fluoro-1,2-dicarba-closo-dodecaborane

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Technology Process of 1-phenyl-2-fluoro-1,2-dicarba-closo-dodecaborane

There total 3 articles about 1-phenyl-2-fluoro-1,2-dicarba-closo-dodecaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 16390-61-7
1-phenyl-1,2-closo-C₂B₁₀H₁₁

: 145490-75-1
N-fluorobenzene sulfonamide

: 778595-92-9
1-phenyl-2-fluoro-1,2-dicarba-closo-dodecaborane

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; under N2 atm. to soln. 1-phenyl-ortho-carborane in Et2O cooled in ice bath was treated with soln. n-BuLi in hexane, allowed to warm slowly to room temp., cooled again, N-fluorobenzenesulfonamide was added; soln. was filtered and washed with water, org. layer was separated, solvent was removed in vacuo, residue was sublimed in vacuo, preparativetlc with cyclohexane as solvent; elem. anal.;
DOI:10.1039/b406422d

Reference yield:

: 16390-61-7
1-phenyl-1,2-closo-C₂B₁₀H₁₁

: 133745-75-2
N-fluorobis(benzenesulfon)imide

: 778595-92-9
1-phenyl-2-fluoro-1,2-dicarba-closo-dodecaborane

Guidance literature:: In benzene; addn. of F compd. in C6H6 to B compd.; L. Droz, Ph. D. Thesis, Charles University, Prague, 2006;
DOI:10.1016/j.molstruc.2010.02.027

Reference yield:

: 41655-52-1
1-lithia-2-phenyl-1,2-dicarba-closo-dodecaborane

: 133745-75-2
N-fluorobis(benzenesulfon)imide

: 778595-92-9
1-phenyl-2-fluoro-1,2-dicarba-closo-dodecaborane

Guidance literature:: In benzene; addn. of F compd. in C6H6 to B compd.; L. Droz, Ph. D. Thesis, Charles University, Prague, 2006;
DOI:10.1016/j.molstruc.2010.02.027