Technology Process of methyl 2-benzyl-6-phenyl-(E)-3-hexenoate
There total 10 articles about methyl 2-benzyl-6-phenyl-(E)-3-hexenoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dipyridinium dichromate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 19h;
DOI:10.1016/j.tet.2006.01.095
- Guidance literature:
-
Multi-step reaction with 3 steps
1: TBAF / tetrahydrofuran / 26 h / 20 °C
2: Dess-Martin periodinane / CH2Cl2; acetonitrile / 3.5 h / 0 - 20 °C
3: 49 mg / PDC / dimethylformamide / 19 h / 20 °C
With
dipyridinium dichromate; tetrabutyl ammonium fluoride; Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2006.01.095
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium amalgam; Na2HPO4 / methanol / 4 h / 0 °C
2: TBAF / tetrahydrofuran / 26 h / 20 °C
3: Dess-Martin periodinane / CH2Cl2; acetonitrile / 3.5 h / 0 - 20 °C
4: 49 mg / PDC / dimethylformamide / 19 h / 20 °C
With
disodium hydrogenphosphate; sodium amalgam; dipyridinium dichromate; tetrabutyl ammonium fluoride; Dess-Martin periodane;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2006.01.095
