(Ru(C₅H₄NCHNC₆H₄CH₃)2Br₂)

Base Information

• Chemical Name: (Ru(C₅H₄NCHNC₆H₄CH₃)2Br₂)
• CAS No.: 146565-02-8
• Molecular Formula: C₂₆H₂₄Br₂N₄Ru
• Molecular Weight: 653.381
• Mol file: 146565-02-8.mol

Synonyms:

Chemical Property of (Ru(C₅H₄NCHNC₆H₄CH₃)2Br₂)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Ru(C₅H₄NCHNC₆H₄CH₃)2Br₂)

There total 1 articles about (Ru(C₅H₄NCHNC₆H₄CH₃)2Br₂) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

pyridine-2-carbaldehyde (1121-60-4) + ruthenium(III) chloride trihydrate (14898-67-0) + p-toluidine (106-49-0,12221-03-3) → (Ru(C5H4NCHNC6H4CH3)2Br2) (146392-93-0,146565-02-8) + (Ru(C5H4NCHNC6H4CH3)2Br2)

Guidance literature:

With lithium bromide; In ethanol; Ru-salt and LiBr are refluxed in EtOH for 15 min, addn. of mixture of organic compounds in EtOH, refluxing for 2 h on a water bath; filtn., washing with EtOH and ether, sepn. of isomers by chromy. on silica gel, eluting with CHCl3/CH3CN, recrystn. from CHCl3/C6H14, filtrate is worked up in a similiar manner to improve the yield, elem. anal. for both isomers;

DOI:10.1016/S0277-5387(00)83661-X

upstream raw materials:

pyridine-2-carbaldehyde

ruthenium(III) chloride trihydrate

p-toluidine