1-ferrocenyl-1-phenylbut-3-ynol

Base Information

Chemical Name:1-ferrocenyl-1-phenylbut-3-ynol
CAS No.:672958-84-8
Molecular Formula:C₂₀H₁₈FeO
Molecular Weight:330.209
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-ferrocenyl-1-phenylbut-3-ynol

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Technology Process of 1-ferrocenyl-1-phenylbut-3-ynol

There total 1 articles about 1-ferrocenyl-1-phenylbut-3-ynol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.8%

: 1272-44-2
benzoylferrocene

: 18295-60-8
propargyl magnesium bromide

: 18295-60-8
allenylmagnesium bromide

: 672958-84-8
1-ferrocenyl-1-phenylbut-3-ynol

Guidance literature:: In diethyl ether; a suspn. of FcCOPh in ether was added within 30 min at -40°C under Ar to an ethereal soln. of the Grignard reagent, the mixt. was allowedto warm to room temp. under stirring; poured onto ice/water, NH4Cl was added, aq. layer was extd. with ether, combined ether phases were washed with water, dried over Na2SO4, evapd. in vacuo; elem. anal.;

Reference yield:

: 672958-84-8
1-ferrocenyl-1-phenylbut-3-ynol

: 74-88-4
methyl iodide

: 672958-85-9
1-ferrocenyl-1-methoxy-1-phenylbut-3-yne

Guidance literature:: With n-butyllithium; In tetrahydrofuran; pentane; a soln. of BuLi in pentane was added at -70°C under Ar to a THF soln. of butynol, the stirred mixt. was allowed to warm to -40°C, MeI was added, the mixt. was stirred overnight at room temp.; water was added, volatiles removed in vacuo, residue was dissolved in ether, soln. washed with water, dried over Na2SO4, evapd., residue was crystd. from hexane; elem. anal.;