methyl 2-allyl-2-MIDA boryl phenyl acetate

Base Information

Chemical Name:methyl 2-allyl-2-MIDA boryl phenyl acetate
CAS No.:1401572-38-0
Molecular Formula:C₁₇H₂₀BNO₆
Molecular Weight:345.16
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-allyl-2-MIDA boryl phenyl acetate

Chemical Property:

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Technology Process of methyl 2-allyl-2-MIDA boryl phenyl acetate

There total 3 articles about methyl 2-allyl-2-MIDA boryl phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1380504-40-4
α-allyl-α-MIDA boryl phenyl acetic acid

: 1401572-38-0
methyl 2-allyl-2-MIDA boryl phenyl acetate

Guidance literature:: With diazomethyl-trimethyl-silane; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/c2ob26503f

Reference yield:

: 1329422-26-5
N-methyliminodiacetyl (2-oxo-1-phenylethyl)boronate

: 1401572-38-0
methyl 2-allyl-2-MIDA boryl phenyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triethyl borane / tetrahydrofuran / 48 h / 50 °C / Molecular sieve; Inert atmosphere; Sealed tube

2: sodium chlorite; sodium dihydrogenphosphate; cyclohexene / tert-butyl alcohol; water / 40 °C

3: diazomethyl-trimethyl-silane / dichloromethane / 2 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethyl borane; triethylamine; cyclohexene; diazomethyl-trimethyl-silane; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c2ob26503f

Reference yield:

: 1380504-39-1
α-allyl-α-MIDA boryl phenyl acetaldehyde

: 1401572-38-0
methyl 2-allyl-2-MIDA boryl phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium chlorite; sodium dihydrogenphosphate; cyclohexene / tert-butyl alcohol; water / 40 °C

2: diazomethyl-trimethyl-silane / dichloromethane / 2 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; cyclohexene; diazomethyl-trimethyl-silane; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c2ob26503f