2,2'-oxybis-3-m-tolyl-4-phenyl-1,3,5,2-oxadiazoborole

Base Information

Chemical Name:2,2'-oxybis-3-m-tolyl-4-phenyl-1,3,5,2-oxadiazoborole
CAS No.:76541-31-6
Molecular Formula:C₂₈H₂₄B₂N₄O₃
Molecular Weight:486.146
Hs Code.:

Synonyms:

Suppliers and Price of 2,2'-oxybis-3-m-tolyl-4-phenyl-1,3,5,2-oxadiazoborole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,2'-oxybis-3-m-tolyl-4-phenyl-1,3,5,2-oxadiazoborole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2'-oxybis-3-m-tolyl-4-phenyl-1,3,5,2-oxadiazoborole

There total 1 articles about 2,2'-oxybis-3-m-tolyl-4-phenyl-1,3,5,2-oxadiazoborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36954-12-8
N-(3-methylphenyl)-benzylamine oxime

: 11113-50-1,14635-83-7
boric acid

: 76541-31-6
2,2'-oxybis-3-m-tolyl-4-phenyl-1,3,5,2-oxadiazoborole

Guidance literature:: In benzene; byproducts: H2O; addn. of boric acid to a benzene soln. of ligand, refluxing for 12 h under exclusion of moisture; removing water water azeotropically with benzene, removal of solvent under reduced pressure, elem. anal.;

Reference yield: 90.0%

: 75-77-4
chloro-trimethyl-silane

: 76541-31-6
2,2'-oxybis-3-m-tolyl-4-phenyl-1,3,5,2-oxadiazoborole

: 76541-34-9
2-trimethylsiloxy-3-m-tolyl-4-phenyl-1,3,5,2-oxadiazaborole

Guidance literature:: With water; triethylamine; In tetrahydrofuran; benzene; byproducts: (C2H5)3NHCl; addn. of an equimolar quantity of water in THF to borole-compd. in benzene, stirring for 10 h at 30°C, addn. of NEt3 and Me3SiCl, stirring for 10 h under exclusion of moisture; filtn., removal of excess solvent from filtrate under vacuo gives viscous compd., solidificationon standing for a few days, elem. anal.;