(C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2⁽¹⁺⁾*BF₄^(1-)=(C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2BF₄

Base Information

Chemical Name:(C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2⁽¹⁺⁾*BF₄^(1-)=(C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2BF₄
CAS No.:686744-76-3
Molecular Formula:BF₄*C₃₇H₃₃Fe₂
Molecular Weight:676.168
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>FeC<sub>5</sub>H<sub>4</sub>)2C<sub>3</sub>H(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)2<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>=(C<sub>5</sub>H<sub>5</sub>FeC<sub>5</sub>H<sub>4</sub>)2C<sub>3</sub>H(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)2BF<sub>4</sub>

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Chemical Property of (C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2⁽¹⁺⁾*BF₄^(1-)=(C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2BF₄

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Technology Process of (C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2⁽¹⁺⁾*BF₄^(1-)=(C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2BF₄

There total 1 articles about (C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2⁽¹⁺⁾*BF₄^(1-)=(C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 686744-66-1
3,3-dibenzyl-1,2-diferrocenylcyclopropene

: 686744-76-3
(C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2⁽¹⁺⁾*BF₄^(1-)=(C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2BF₄

Guidance literature:: In diethyl ether; (N2); dropwise addn. of acid to a soln. of iron complex in Et2O at -50°C, stirring for 15 min at -50°C; decantation, washing with cold Et2O, drying in vac. with cooling;
DOI:10.1039/b307408k

Reference yield: 72.0%

: 686744-76-3
(C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2⁽¹⁺⁾*BF₄^(1-)=(C₅H₅FeC₅H₄)2C₃H(CH₂C₆H₅)2BF₄

: 1,1-dibenzyl-2,3-diferrocenylallylium tetrafluoroborate

Guidance literature:: In dichloromethane; keeping a soln. of iron complex in CH2Cl2 at room temp. for 4 h; addn. of Et2O, filtration of ppt., washing with ether, drying in vac.; elem. anal.;
DOI:10.1039/b307408k