[(N(C₂H₄NSi(CH₃)3)3)Zr(As(C₆H₅)2)]

Base Information

Chemical Name:[(N(C₂H₄NSi(CH₃)3)3)Zr(As(C₆H₅)2)]
CAS No.:1069138-24-4
Molecular Formula:C₂₇H₄₉AsN₄Si₃Zr
Molecular Weight:680.115
Hs Code.:

[(N(C<sub>2</sub>H<sub>4</sub>NSi(CH<sub>3</sub>)3)3)Zr(As(C<sub>6</sub>H<sub>5</sub>)2)]

Synonyms:

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Chemical Property of [(N(C₂H₄NSi(CH₃)3)3)Zr(As(C₆H₅)2)]

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Technology Process of [(N(C₂H₄NSi(CH₃)3)3)Zr(As(C₆H₅)2)]

There total 1 articles about [(N(C₂H₄NSi(CH₃)3)3)Zr(As(C₆H₅)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 937801-07-5
[κ⁵-N,N,N,N,C-(Me₃SiNCH₂CH₂)₂NCH₂CH₂NSiMe₂CH₂]Zr

: 829-83-4
diphenylarsane

: 1069138-24-4
[(N(C₂H₄NSi(CH₃)3)3)Zr(As(C₆H₅)2)]

Guidance literature:: In diethyl ether; (N2); Schlenk technique; cold. soln. of As compd. in Et2O was added dropwise to soln. of Zr complex in Et2O at -30°C; stirred at ambient temp. for 15 min; Et2O removed (vac.); recrystd. (Et2O, low temp.); elem. anal.;
DOI:10.1039/b718050k

Reference yield: 86.0%

: 1069138-24-4
[(N(C₂H₄NSi(CH₃)3)3)Zr(As(C₆H₅)2)]

: 100-47-0
benzonitrile

: 1069138-32-4
[(N(CH₂CH₂NSiMe₃)3)Zr(N=CPh(AsPh₂))]

Guidance literature:: In benzene; (N2); Schlenk technique; soln. of nitrile in C6H6 was added to soln. of Zr complex in C6H6 at ambient temp.; reacted for 20 min; frozen; lyophilized; dissolved in Et2O; filtered; cooled to -30°Cfor 2 d; elem. anal.;
DOI:10.1039/b718050k

Reference yield: 72.0%

: 1069138-24-4
[(N(C₂H₄NSi(CH₃)3)3)Zr(As(C₆H₅)2)]

: 88333-03-3,10340-91-7
Benzyl isocyanide

: 1069138-31-3
[(N(CH₂CH₂NSiMe₃)3)Zr(C(AsPh₂)=NCH₂Ph)]

Guidance literature:: In benzene; (N2); Schlenk technique; soln. of isocyanide in C6H6 was added to soln. of Zr complex in C6H6 at ambient temp.; reacted for 15 min; frozen; lyophilized; dissolved in Et2O; filtered through Celite; cooled to -30°C for 2 d; elem. anal.;
DOI:10.1039/b718050k