Technology Process of N,N,N',N'-tetra(2-pyridyl)-1,1-biphenyl-4,4'-diamine
There total 1 articles about N,N,N',N'-tetra(2-pyridyl)-1,1-biphenyl-4,4'-diamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(II) sulfate; potassium hydroxide;
at 180 ℃;
for 8h;
Inert atmosphere;
DOI:10.1039/c7gc00503b
- Guidance literature:
-
In
tetrahydrofuran; dichloromethane;
ligand and Pt-complex were dissolved in THF/CH2Cl2, stirred for 10 min; filtered, toluene was slowly added, solvent was allowed to diffuse, evapd. slowly over 2 d at ambient temp.; elem. anal.;
DOI:10.1021/om030262k
- Guidance literature:
-
In
water;
High Pressure; mixt. CuI, ligand and water in sealed Teflon-lined reactor was heated at180°C for 3 days; react. mixt. was slowly cooled to room temp., washed with water and EtOHand dried in air; elem. anal.;
DOI:10.1039/c2dt12032a
