fac-[Mn(CNPh)(CO)3(bis(dimethylphosphino)methane)]ClO₄

Base Information

Chemical Name:fac-[Mn(CNPh)(CO)3(bis(dimethylphosphino)methane)]ClO₄
CAS No.:628692-43-3
Molecular Formula:C₁₅H₁₉MnNO₃P₂*ClO₄
Molecular Weight:477.657
Hs Code.:

fac-[Mn(CNPh)(CO)3(bis(dimethylphosphino)methane)]ClO<sub>4</sub>

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Chemical Property of fac-[Mn(CNPh)(CO)3(bis(dimethylphosphino)methane)]ClO₄

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Technology Process of fac-[Mn(CNPh)(CO)3(bis(dimethylphosphino)methane)]ClO₄

There total 1 articles about fac-[Mn(CNPh)(CO)3(bis(dimethylphosphino)methane)]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 914365-07-4
fac-[Mn(OClO₃)(CO)3(bis(dimethylphosphino)methane)]

: 1197040-29-1,931-54-4
phenyl isocyanate

: 628692-43-3
fac-[Mn(CNPh)(CO)3(bis(dimethylphosphino)methane)]ClO₄

Guidance literature:: In dichloromethane; under N2; addn. of phenylisonitrile to soln. of manganese compd. in CH2Cl2, stirring for 12 h; evapn. under vac., residue washed with hexane and Et2O; elem. anal.;
DOI:10.1039/b607839g

Reference yield: 88.0%

: 628692-43-3
fac-[Mn(CNPh)(CO)3(bis(dimethylphosphino)methane)]ClO₄

: potassium hydroxide

: fac-[Mn(CNPh)(CO)3(PMe₂O)(PMe₃)]

Guidance literature:: In dichloromethane; under N2; excess of KOH added to soln. of Mn compd. in CH2Cl2, stirring for 1.5 h; filtration, filtrate concd., addn. of hexane, solid filtered off and dried; elem. anal.;
DOI:10.1039/b607839g

Reference yield: 70.0%

: 67-56-1
methanol

: 628692-43-3
fac-[Mn(CNPh)(CO)3(bis(dimethylphosphino)methane)]ClO₄

: fac-[Mn(CNPh)(CO)3(PMe₃)(PMe₂OMe))]ClO₄

Guidance literature:: With CH₃ONa; In methanol; under N2; soln. of sodium methoxide in methanol added to soln. of manganese compd. in CH2Cl2, stirring for 1.5 h; filtration, filtrate concd., addn. of Et2O, solid filtered off and dried; elem. anal.;
DOI:10.1039/b607839g