C₂₁H₃₂O₂Si

Base Information

Chemical Name:C₂₁H₃₂O₂Si
CAS No.:1580522-82-2
Molecular Formula:C₂₁H₃₂O₂Si
Molecular Weight:344.569
Hs Code.:

C<sub>21</sub>H<sub>32</sub>O<sub>2</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₃₂O₂Si

Chemical Property:

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Technology Process of C₂₁H₃₂O₂Si

There total 6 articles about C₂₁H₃₂O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1580522-82-2
C₂₁H₃₂O₂Si

Guidance literature:: Multi-step reaction with 4 steps

1: 1H-imidazole; dmap / dichloromethane / 16 h / 20 °C / Inert atmosphere

2: potassium carbonate / methanol / 2 h / 20 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 72 h / -25 °C / Inert atmosphere

4: dichloromethane / 72 h / -25 °C / Inert atmosphere

With 1H-imidazole; dmap; potassium carbonate; Dess-Martin periodane; In methanol; dichloromethane;
DOI:10.1002/anie.201309162

Reference yield:

: 1580522-65-1
C₁₈H₂₈O₂Si

: 1580522-82-2
C₂₁H₃₂O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane / 72 h / -25 °C / Inert atmosphere

2: dichloromethane / 72 h / -25 °C / Inert atmosphere

With Dess-Martin periodane; In dichloromethane;
DOI:10.1002/anie.201309162

Reference yield:

: C₂₀H₃₀O₃Si

: 1580522-82-2
C₂₁H₃₂O₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / methanol / 2 h / 20 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 72 h / -25 °C / Inert atmosphere

3: dichloromethane / 72 h / -25 °C / Inert atmosphere

With potassium carbonate; Dess-Martin periodane; In methanol; dichloromethane;
DOI:10.1002/anie.201309162