N-Cbz-5-thioketone-(S)-tert-butylpipecolate trimer

Base Information

Chemical Name:N-Cbz-5-thioketone-(S)-tert-butylpipecolate trimer
CAS No.:1356411-83-0
Molecular Formula:C₅₄H₆₉N₃O₁₂S₃
Molecular Weight:1048.35
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Cbz-5-thioketone-(S)-tert-butylpipecolate trimer

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Technology Process of N-Cbz-5-thioketone-(S)-tert-butylpipecolate trimer

There total 1 articles about N-Cbz-5-thioketone-(S)-tert-butylpipecolate trimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

: 147489-30-3
(2S)-5-oxopiperidine-1,2-dicarboxylic acid 1-benzyl ester 2-tert-butyl ester

: 1356383-48-6
N-Cbz-5,6-dehydro-5-thiol-tert-butyl-(S)-pipecolate

: 1356411-83-0
N-Cbz-5-thioketone-(S)-tert-butylpipecolate trimer

Guidance literature:: With morpholine; hydrogen sulfide; In N,N-dimethyl-formamide; at 10 ℃; for 5h; Inert atmosphere;
DOI:10.1039/c0mb00227e

Reference yield:

: 1356411-83-0
N-Cbz-5-thioketone-(S)-tert-butylpipecolate trimer

: 501-53-1,94274-21-2
benzyl chloroformate

: 121-45-9
phosphorous acid trimethyl ester

: 1356383-51-1
N-Cbz-5-dimethylphosphonate-(S)-tert-butylpipecolate

Guidance literature:: N-Cbz-5-thioketone-(S)-tert-butylpipecolate trimer; phosphorous acid trimethyl ester; In toluene; for 40h; Inert atmosphere; Reflux;

In ethanol; water; for 2h; Inert atmosphere;

benzyl chloroformate; With N-ethyl-N,N-diisopropylamine; at 0 - 20 ℃;
DOI:10.1039/c0mb00227e