N,N,N'-tris(trimethylsilyl)benzamidine

Base Information

• Chemical Name: N,N,N'-tris(trimethylsilyl)benzamidine
• CAS No.: 119921-07-2
• Molecular Formula: C₁₃H₂₄N₂Si₂
• Molecular Weight: 264.518

Synonyms:

Chemical Property of N,N,N'-tris(trimethylsilyl)benzamidine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of N,N,N'-tris(trimethylsilyl)benzamidine

There total 1 articles about N,N,N'-tris(trimethylsilyl)benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N,N,N'-tris(trimethylsilyl)benzamidine (119921-07-2)

Guidance literature:

Lsg. von NaN2, 1) Benzamid, sd. Bzl., 2) (CH3)3SiCl, neben N-Trimethylsilyl-benzimidsaeure-trimethylsilylester;

Reference yield: 90.0%

N,N,N'-tris(trimethylsilyl)benzamidine (119921-07-2) + boron tribromide (10294-33-4) → (N,N'-bis-(trimethylsilyl)benzamidinato)BBr2

Guidance literature:

In further solvent(s); byproducts: Me3SiBr; (Ar); std. Schlenk technique; soln. of BBr3 (1 equiv.) in CH2Br2 was added to stirred soln. of ligand (1 equiv.) in CH2Br2 at room temp.; mixt. was warmed to 45°C for several min; cooled to room temp. and stirred for 6 h; concd. (vac.); storage at -30°C; filtered; filtrate cooled to -30°C;

DOI:10.1039/b509392a

Reference yield: 84.0%

N,N,N'-tris(trimethylsilyl)benzamidine (119921-07-2) + boron trichloride (10294-34-5) → [C6H5C(N(Si(CH3)3))2]BCl2

Guidance literature:

In dichloromethane; byproducts: Me3SiCl; (Ar); std. Schlenk technique; soln. of BCl3 (1 equiv.) in CH2Cl2 was added to stirred soln. of ligand (1 equiv.) in CH2Br2 at room temp.; mixt. was warmed to 45°C for several min; cooled to room temp. and stirred for 6 h; concd. (vac.); storage at -30°C; filtered; filtrate cooled to -30°C;

DOI:10.1039/b509392a

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