trans-carbonylchlorobis((2-ethylphenyl)-diphenylphosphine)rhodium(I)

Base Information

Chemical Name:trans-carbonylchlorobis((2-ethylphenyl)-diphenylphosphine)rhodium(I)
CAS No.:125852-38-2
Molecular Formula:C₄₁H₃₈ClOP₂Rh
Molecular Weight:747.058
Hs Code.:

Synonyms:

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Chemical Property of trans-carbonylchlorobis((2-ethylphenyl)-diphenylphosphine)rhodium(I)

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Technology Process of trans-carbonylchlorobis((2-ethylphenyl)-diphenylphosphine)rhodium(I)

There total 2 articles about trans-carbonylchlorobis((2-ethylphenyl)-diphenylphosphine)rhodium(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62318-76-7
{Rh((o-vinylphenyl)-diphenylphosphine)2}BF₄

: 51008-43-6
[2-(ethyl)phenyl]-(diphenyl) phosphane

: 125852-38-2
trans-carbonylchlorobis((2-ethylphenyl)-diphenylphosphine)rhodium(I)

Guidance literature:: With formaldehyd; lithium chloride; In tetrahydrofuran; methanol; under N2 or Ar; addn. of 10-fold excess of paraformaldehyde to soln. of Rh-complex in THF, refluxing (1 h), pptn. on addn. of LiCl in MeOH;
DOI:10.1016/S0277-5387(00)80356-3

Reference yield:

: di(rhodium)tetracarbonyl dichloride

: 51008-43-6
[2-(ethyl)phenyl]-(diphenyl) phosphane

: 125852-38-2
trans-carbonylchlorobis((2-ethylphenyl)-diphenylphosphine)rhodium(I)

Guidance literature:: In benzene; under N2 or Ar; dropwise addn. of soln. of org. compd. to soln. of Rh-complex in benzene, pptn.;
DOI:10.1016/S0277-5387(00)80356-3

Reference yield:

: 14104-20-2
silver tetrafluoroborate

: 125852-38-2
trans-carbonylchlorobis((2-ethylphenyl)-diphenylphosphine)rhodium(I)

: {Rh(carbonyl)(acetonitrile)((2-ethylphenyl)-diphenylphosphine)2}BF₄

Guidance literature:: In [D₃]acetonitrile; acetonitrile; byproducts: AgCl; under N2 or Ar; addn. of soln. of Ag-complex to soln. of Rh-complex in CH3CN or CD3CN; AgCl removal (centrifugation), solvent evapn.; elem. anal.;
DOI:10.1016/S0277-5387(00)80356-3