(4S)-4a,7t,10ξ-trimethyl-2-phenyl-(4ac,6at,9ac)-4,4a,5,6,6a,9a-hexahydro-7H-4r,9bc-propano-furo[2',3':3,4]benzo[1,2-e][1,3]oxazine-8,11-dion 11-oxime

Base Information

Chemical Name:(4S)-4a,7t,10ξ-trimethyl-2-phenyl-(4ac,6at,9ac)-4,4a,5,6,6a,9a-hexahydro-7H-4r,9bc-propano-furo[2',3':3,4]benzo[1,2-e][1,3]oxazine-8,11-dion 11-oxime
CAS No.:64234-88-4
Molecular Formula:C₂₂H₂₆N₂O₄
Molecular Weight:382.459
Hs Code.:

(4<i>S</i>)-4a,7<i>t</i>,10ξ-trimethyl-2-phenyl-(4a<i>c</i>,6a<i>t</i>,9a<i>c</i>)-4,4a,5,6,6a,9a-hexahydro-7<i>H</i>-4<i>r</i>,9b<i>c</i>-propano-furo[2',3':3,4]benzo[1,2-<i>e</i>][1,3]oxazine-8,11-dion 11-oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S)-4a,7t,10ξ-trimethyl-2-phenyl-(4ac,6at,9ac)-4,4a,5,6,6a,9a-hexahydro-7H-4r,9bc-propano-furo[2',3':3,4]benzo[1,2-e][1,3]oxazine-8,11-dion 11-oxime

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Technology Process of (4S)-4a,7t,10ξ-trimethyl-2-phenyl-(4ac,6at,9ac)-4,4a,5,6,6a,9a-hexahydro-7H-4r,9bc-propano-furo[2',3':3,4]benzo[1,2-e][1,3]oxazine-8,11-dion 11-oxime

There total 4 articles about (4S)-4a,7t,10ξ-trimethyl-2-phenyl-(4ac,6at,9ac)-4,4a,5,6,6a,9a-hexahydro-7H-4r,9bc-propano-furo[2',3':3,4]benzo[1,2-e][1,3]oxazine-8,11-dion 11-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 481-06-1
santonin

: 64201-54-3,64234-86-2,64234-87-3,64234-88-4
(4S)-4a,7t,10ξ-trimethyl-2-phenyl-(4ac,6at,9ac)-4,4a,5,6,6a,9a-hexahydro-7H-4r,9bc-propano-furo[2',3':3,4]benzo[1,2-e][1,3]oxazine-8,11-dion 11-oxime

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe, NH₂OH*HCl / methanol

2: ethanol

With hydroxylamine hydrochloride; sodium methylate; In methanol; ethanol;
DOI:10.1021/jo00398a002