cct-RuCl₂(CO)2(1-phenyl-3,4-dimethylphosphole)2

Base Information

Chemical Name:cct-RuCl₂(CO)2(1-phenyl-3,4-dimethylphosphole)2
CAS No.:86421-54-7
Molecular Formula:C₂₆H₂₆Cl₂O₂P₂Ru
Molecular Weight:604.415
Hs Code.:

cct-RuCl<sub>2</sub>(CO)2(1-phenyl-3,4-dimethylphosphole)2

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Chemical Property of cct-RuCl₂(CO)2(1-phenyl-3,4-dimethylphosphole)2

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Technology Process of cct-RuCl₂(CO)2(1-phenyl-3,4-dimethylphosphole)2

There total 6 articles about cct-RuCl₂(CO)2(1-phenyl-3,4-dimethylphosphole)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 30540-36-4
3,4-dimethyl-1-phenylphosphole

: 86421-54-7,86495-69-4
cct-RuCl₂(CO)2(1-phenyl-3,4-dimethylphosphole)2

Guidance literature:: With carbon monoxide; In 2-methoxy-ethanol; a soln. of RuCl3 was refluxed when CO was bubbled through it for 5 h, then phosphole was added to the soln.; filtration, ppt. was washed with diethyl ether,; elem. anal.;

Reference yield: 36.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 30540-36-4
3,4-dimethyl-1-phenylphosphole

: 86421-54-7,86495-69-4
trans, trans, trans-dichlorodicarbonylbis(1-phenyl-3,4-dimethylphosphole)ruthenium(II)

Guidance literature:: With carbon monoxide; In 2-methoxy-ethanol; refluxing in 2-methoxyethanol with CO refluxing through; cooled to 0°C; ligand added;; addn. of H2O; crystn.; elem. anal.;;
DOI:10.1021/ic00319a017

Reference yield:

: 14898-67-0
ruthenium(III) chloride trihydrate

: 30540-36-4
3,4-dimethyl-1-phenylphosphole

: 86421-54-7,86495-69-4
trans, trans, trans-dichlorodicarbonylbis(1-phenyl-3,4-dimethylphosphole)ruthenium(II)

: 86421-54-7,86495-69-4
ccc-RuCl₂(CO)2(1-phenyl-3,4-dimethylphosphole)2

: 86421-54-7,86495-69-4
cct-RuCl₂(CO)2(1-phenyl-3,4-dimethylphosphole)2

Guidance literature:: With carbon monoxide; In 2-methoxy-ethanol; refluxing in 2-methoxyethanol with CO refluxing through; ligand added; at 60°C the major product is the ccc-isomer;
DOI:10.1021/ic00319a017