(1,2,5,6-η4-cyclooctadiene)bis(2,4-dinitrophenyl)platinum(II)

Base Information

Chemical Name:(1,2,5,6-η4-cyclooctadiene)bis(2,4-dinitrophenyl)platinum(II)
CAS No.:100229-02-5
Molecular Formula:C₂₀H₁₈N₄O₈Pt
Molecular Weight:637.465
Hs Code.:

Synonyms:

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Chemical Property of (1,2,5,6-η4-cyclooctadiene)bis(2,4-dinitrophenyl)platinum(II)

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Technology Process of (1,2,5,6-η4-cyclooctadiene)bis(2,4-dinitrophenyl)platinum(II)

There total 3 articles about (1,2,5,6-η4-cyclooctadiene)bis(2,4-dinitrophenyl)platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 709-49-9
1-iodo-2,4-dinitrobenzene

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 591-51-5
phenyllithium

: 100229-02-5
(1,2,5,6-η4-cyclooctadiene)bis(2,4-dinitrophenyl)platinum(II)

Guidance literature:: With carbon dioxide; In tetrahydrofuran; (Ar); Pt-complex added to PhLi and IC6H3(NO2)2 in THF in small portions, temp. held below -100°C; mixt. stirred at -105°C for 5 h; dry CO2 bubbled through soln. for 15 min; mixt. warmed to room temp.; addn. of water, extn. (CH2Cl2); solvent removed in vac.; soln. layered with petroleum ether, stored 24 h at -20°C, elem. anal.;

Reference yield:

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 76074-20-9
1-trimethylstannyl-2,4-dinitrobenzene

: 100229-04-7
chloro(1,2,5,6-η4-cyclooctadiene)(2,4-dinitrophenyl)platinum(II)

: 100229-02-5
(1,2,5,6-η4-cyclooctadiene)bis(2,4-dinitrophenyl)platinum(II)

Guidance literature:: In further solvent(s); stannane added to the Pt-complex in 1,1,2,2-tetrachloroethane, mixt. heated for 20 h at 100°C; solvent removed, residue dissolved in CH2Cl2; soln. layered with methanol, stored for 24 h at -20°C, chromy. (SiO2, CH2Cl2), elem. anal.; yield depends on concn. of the educts;