Technology Process of 10,11,12,13-Tetraphenyl-3-oxatricyclo<7.4.0.02,4>trideca-1(9),10,12-trien
There total 7 articles about 10,11,12,13-Tetraphenyl-3-oxatricyclo<7.4.0.02,4>trideca-1(9),10,12-trien which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
toluene;
1.) 30 min, room temp.; 2.) 30 min, reflux;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 77 percent / 90percent m-chloroperbenzoic acid / CH2Cl2 / 5 h / -5 - 5 °C
2: 54 percent / 1.) sodium acetate / ethanol / 1.) reflux; 2.) 5 min, reflux
3: 20 percent / SeO2 / dioxane / 52 h
4: 17 percent / Cu-powder / 180 °C / 1 - 7.5 Torr
5: 85 percent / toluene / 1.) 30 min, room temp.; 2.) 30 min, reflux
With
selenium(IV) oxide; sodium acetate; copper; 3-chloro-benzenecarboperoxoic acid;
In
1,4-dioxane; ethanol; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 41 percent / CrO3/H2SO4
2: 77 percent / 90percent m-chloroperbenzoic acid / CH2Cl2 / 5 h / -5 - 5 °C
3: 54 percent / 1.) sodium acetate / ethanol / 1.) reflux; 2.) 5 min, reflux
4: 20 percent / SeO2 / dioxane / 52 h
5: 17 percent / Cu-powder / 180 °C / 1 - 7.5 Torr
6: 85 percent / toluene / 1.) 30 min, room temp.; 2.) 30 min, reflux
With
chromium(VI) oxide; selenium(IV) oxide; sulfuric acid; sodium acetate; copper; 3-chloro-benzenecarboperoxoic acid;
In
1,4-dioxane; ethanol; dichloromethane; toluene;
