(meso-tetra-p-tolylporphyrinato)MoCl₂

Base Information

Chemical Name:(meso-tetra-p-tolylporphyrinato)MoCl₂
CAS No.:64024-40-4
Molecular Formula:C₄₈H₃₆Cl₂MoN₄
Molecular Weight:835.687
Hs Code.:

(meso-tetra-p-tolylporphyrinato)MoCl<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (meso-tetra-p-tolylporphyrinato)MoCl₂

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Technology Process of (meso-tetra-p-tolylporphyrinato)MoCl₂

There total 1 articles about (meso-tetra-p-tolylporphyrinato)MoCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 5,10,15,20-tetra-p-tolylporphyrin, dilithium salt * 2 THF

: 56613-96-8,77210-60-7,15584-93-7,19187-82-7
bis(acetonitrile)tetrachloromolybdenum(IV)

: 64024-40-4
(meso-tetra-p-tolylporphyrinato)MoCl₂

Guidance literature:: In toluene; byproducts: LiCl, THF; inetr atmosphere; stirring and mild heating (12 h); cooling to room temp., filtration, evapn., dissoln. in CH2Cl2, filtration, evapn., crystn. (CH2Cl2 : hexane = 1:3);

Reference yield: 60.0%

: 64024-40-4
(meso-tetra-p-tolylporphyrinato)MoCl₂

: 20732-26-7,82959-02-2
lithium anilide

: 868666-02-8
(meso-tetra-p-tolylporphyrinato)Mo=NC₆H₅

Guidance literature:: In toluene; byproducts: LiCl, H2NC6H5; anerobic treatment; recrystn. (toluene/hexane, -20°C, 1 h), filtration, washing (hexanes), drying (vac.);
DOI:10.1021/ic051100e

Reference yield: 50.0%

: 64024-40-4
(meso-tetra-p-tolylporphyrinato)MoCl₂

: 64024-42-6
Mo(IV)(O)(ttp)

: 91156-35-3
cis-(meso-tetra-p-tolylporphyrinato)Mo(CO)2

Guidance literature:: With CO; zinc amalgam; In benzene; CO was bubbled in a benzene soln. of the Mo complex in presence of Zn amalgam, stirred overnight at room temp. under 1.5 atm CO; filtered, evapd. to dryness, crystd. from mesitylene-heptane in darkness under CO;