(2,6-dibromo-4-tert-butylphenyl)(2-iodo-4-tert-butylphenyl)methyl methyl eter

Base Information

Chemical Name:(2,6-dibromo-4-tert-butylphenyl)(2-iodo-4-tert-butylphenyl)methyl methyl eter
CAS No.:1227674-47-6
Molecular Formula:C₂₂H₂₇Br₂IO
Molecular Weight:594.168
Hs Code.:

Synonyms:

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Chemical Property of (2,6-dibromo-4-tert-butylphenyl)(2-iodo-4-tert-butylphenyl)methyl methyl eter

Chemical Property:

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Technology Process of (2,6-dibromo-4-tert-butylphenyl)(2-iodo-4-tert-butylphenyl)methyl methyl eter

There total 10 articles about (2,6-dibromo-4-tert-butylphenyl)(2-iodo-4-tert-butylphenyl)methyl methyl eter which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1227674-40-9
ethyl N-nitroso-N-[(2,6-dibromo-4-tert-butylphenyl)(2,6-diiodo-4-tert-butylphenyl)methyl]carbamate

: 1227674-47-6
(2,6-dibromo-4-tert-butylphenyl)(2-iodo-4-tert-butylphenyl)methyl methyl eter

: 1227674-46-5
C₂₂H₂₆Br₂I₂O

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / -15 - 20 °C / Inert atmosphere

2: benzene / 25 °C / Photolysis

With potassium tert-butylate; In tetrahydrofuran; benzene;
DOI:10.1002/poc.1651

Reference yield:

: 1227674-36-3
4-tert-butyl-2,6-diiodobenzaldehyde

: 1227674-47-6
(2,6-dibromo-4-tert-butylphenyl)(2-iodo-4-tert-butylphenyl)methyl methyl eter

: 1227674-46-5
C₂₂H₂₆Br₂I₂O

Guidance literature:: Multi-step reaction with 6 steps

1.1: n-butyllithium / diethyl ether; hexane / 5 h / -78 °C

1.2: -78 - 20 °C

2.1: thionyl chloride / 20 °C

3.1: silver tetrafluoroborate / 1,4-dioxane / 60 - 100 °C

4.1: acetic anhydride; acetic acid; sodium nitrite / 0 - 20 °C

5.1: potassium tert-butylate / tetrahydrofuran / -15 - 20 °C / Inert atmosphere

6.1: benzene / 25 °C / Photolysis

With silver tetrafluoroborate; n-butyllithium; thionyl chloride; potassium tert-butylate; acetic anhydride; acetic acid; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; benzene;
DOI:10.1002/poc.1651

Reference yield:

: 1227674-34-1
4-tert-butyl-2,6-diiodobenzyl acetate

: 1227674-47-6
(2,6-dibromo-4-tert-butylphenyl)(2-iodo-4-tert-butylphenyl)methyl methyl eter

: 1227674-46-5
C₂₂H₂₆Br₂I₂O

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / methanol / 3 h / 20 °C

2.1: pyridinium chlorochromate / dichloromethane / 20 °C

3.1: n-butyllithium / diethyl ether; hexane / 5 h / -78 °C

3.2: -78 - 20 °C

4.1: thionyl chloride / 20 °C

5.1: silver tetrafluoroborate / 1,4-dioxane / 60 - 100 °C

6.1: acetic anhydride; acetic acid; sodium nitrite / 0 - 20 °C

7.1: potassium tert-butylate / tetrahydrofuran / -15 - 20 °C / Inert atmosphere

8.1: benzene / 25 °C / Photolysis

With silver tetrafluoroborate; n-butyllithium; thionyl chloride; potassium tert-butylate; acetic anhydride; potassium carbonate; acetic acid; pyridinium chlorochromate; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; hexane; dichloromethane; benzene;
DOI:10.1002/poc.1651