C₂₁H₂₆N₂O₄S

Base Information

Chemical Name:C₂₁H₂₆N₂O₄S
CAS No.:1360464-25-0
Molecular Formula:C₂₁H₂₆N₂O₄S
Molecular Weight:402.514
Hs Code.:

C<sub>21</sub>H<sub>26</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₆N₂O₄S

Chemical Property:

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Technology Process of C₂₁H₂₆N₂O₄S

There total 10 articles about C₂₁H₂₆N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1360464-28-3
C₂₁H₂₃NO₅S

: 1360464-25-0
C₂₁H₂₆N₂O₄S

Guidance literature:: With ammonia; sodium tris(acetoxy)borohydride; In 1,4-dioxane;
DOI:10.1016/j.bmcl.2011.12.057

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1360464-25-0
C₂₁H₂₆N₂O₄S

Guidance literature:: Multi-step reaction with 11 steps

1: sodium hydride / tetrahydrofuran / Reflux

2: ytterbium(III) triflate / benzene / Reflux

3: sodium tris(acetoxy)borohydride; acetic acid / acetonitrile

4: sodium t-butanolate / tetrahydrofuran

5: lithium aluminium tetrahydride / diethyl ether

6: 20% palladium hydroxide on charcoal; hydrogen / methanol

7: potassium carbonate / dichloromethane

8: tributylphosphine / acetonitrile

9: 3-chloro-benzenecarboperoxoic acid / dichloromethane

10: hydrogenchloride / acetone / Reflux

11: ammonia; sodium tris(acetoxy)borohydride / 1,4-dioxane

With hydrogenchloride; lithium aluminium tetrahydride; tributylphosphine; 20% palladium hydroxide on charcoal; ammonia; hydrogen; sodium tris(acetoxy)borohydride; sodium hydride; potassium carbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; sodium t-butanolate; ytterbium(III) triflate; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane; acetone; acetonitrile; benzene;
DOI:10.1016/j.bmcl.2011.12.057

Reference yield:

: 813445-20-4
(7R,8R)-8-((R)-1-phenyl-ethylamino)-1,4-dioxa-spiro[4.5]decane-7-carboxylic acid ethyl ester

: 1360464-25-0
C₂₁H₂₆N₂O₄S

Guidance literature:: Multi-step reaction with 7 steps

1: lithium aluminium tetrahydride / diethyl ether

2: 20% palladium hydroxide on charcoal; hydrogen / methanol

3: potassium carbonate / dichloromethane

4: tributylphosphine / acetonitrile

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane

6: hydrogenchloride / acetone / Reflux

7: ammonia; sodium tris(acetoxy)borohydride / 1,4-dioxane

With hydrogenchloride; lithium aluminium tetrahydride; tributylphosphine; 20% palladium hydroxide on charcoal; ammonia; hydrogen; sodium tris(acetoxy)borohydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; methanol; diethyl ether; dichloromethane; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2011.12.057