C₁₄H₁₉ClN₄S

Base Information

• Chemical Name: C₁₄H₁₉ClN₄S
• CAS No.: 1351946-10-5
• Molecular Formula: C₁₄H₁₉ClN₄S
• Molecular Weight: 310.851
• Mol file: 1351946-10-5.mol

Synonyms:

Chemical Property of C₁₄H₁₉ClN₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₉ClN₄S

There total 3 articles about C₁₄H₁₉ClN₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

5-(4-chlorophenyl)-3-mercapto-1,2,4-triazole (26028-65-9) + 2-(diethylamino)ethyl chloride (100-35-6) → C14H19ClN4S (1351946-10-5)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; for 6h; Reflux;

DOI:10.1007/s00044-011-9902-z

Reference yield:

4-chloro-benzoyl chloride (122-01-0) → C14H19ClN4S (1351946-10-5)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine / -5 - 0 °C

2: sodium hydroxide / 4 h / Reflux

3: potassium carbonate; potassium iodide / acetone / 6 h / Reflux

With pyridine; potassium carbonate; potassium iodide; sodium hydroxide; In acetone;

DOI:10.1007/s00044-011-9902-z

Reference yield:

1-(4-chlorobenzoyl)thiosemicarbazide (64310-32-3) → C14H19ClN4S (1351946-10-5)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / 4 h / Reflux

2: potassium carbonate; potassium iodide / acetone / 6 h / Reflux

With potassium carbonate; potassium iodide; sodium hydroxide; In acetone;

DOI:10.1007/s00044-011-9902-z

upstream raw materials:

4-chloro-benzoyl chloride

1-(4-chlorobenzoyl)thiosemicarbazide

5-(4-chlorophenyl)-3-mercapto-1,2,4-triazole

2-(diethylamino)ethyl chloride

Refernces