C₁₈H₁₄OS₂

Base Information

• Chemical Name: C₁₈H₁₄OS₂
• CAS No.: 1379588-81-4
• Molecular Formula: C₁₈H₁₄OS₂
• Molecular Weight: 310.441
• Mol file: 1379588-81-4.mol

Synonyms:

Chemical Property of C₁₈H₁₄OS₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₁₄OS₂

There total 3 articles about C₁₈H₁₄OS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

carbon disulfide (75-15-0,12122-00-8) + 1-(benzyloxy)-4-bromonaphthalene (138865-41-5) → C18H14OS2 (1379588-81-4)

Guidance literature:

1-(benzyloxy)-4-bromonaphthalene; With iodine; magnesium; In tetrahydrofuran; diethyl ether; for 3h; Inert atmosphere; Reflux;

carbon disulfide; In tetrahydrofuran; diethyl ether;

DOI:10.1080/00397911.2011.565142

Reference yield:

α-naphthol (90-15-3) → C18H14OS2 (1379588-81-4)

Guidance literature:

Multi-step reaction with 3 steps

1: N-Bromosuccinimide / acetonitrile

2: potassium carbonate / acetonitrile / 20 - 60 °C

3: iodine; magnesium / tetrahydrofuran; diethyl ether / 3 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; iodine; potassium carbonate; magnesium; In tetrahydrofuran; diethyl ether; acetonitrile;

DOI:10.1080/00397911.2011.565142

Reference yield:

4-bromo-1-naphthol (571-57-3) → C18H14OS2 (1379588-81-4)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 20 - 60 °C

2: iodine; magnesium / tetrahydrofuran; diethyl ether / 3 h / Inert atmosphere; Reflux

With iodine; potassium carbonate; magnesium; In tetrahydrofuran; diethyl ether; acetonitrile;

DOI:10.1080/00397911.2011.565142

upstream raw materials:

carbon disulfide

1-(benzyloxy)-4-bromonaphthalene

α-naphthol

4-bromo-1-naphthol

Downstream raw materials:

C₂₄H₂₅NO₃S

C₂₃H₂₃NO₃S

C₂₅H₁₇NOS₃