(10S)-3c-Hydroxy-10r.13c-dimethyl-17c-((1S:4R)-1.4.5-trimethyl-hexyl)-(5tH.8cH.9tH.14tH)-hexadecahydro-1H-cyclopenta[a]phenanthren

Base Information

• Chemical Name: (10S)-3c-Hydroxy-10r.13c-dimethyl-17c-((1S:4R)-1.4.5-trimethyl-hexyl)-(5tH.8cH.9tH.14tH)-hexadecahydro-1H-cyclopenta[a]phenanthren
• CAS No.: 17105-72-5
• Molecular Formula: C₂₈H₅₀O
• Molecular Weight: 402.704
• Mol file: 17105-72-5.mol

Synonyms:

Chemical Property of (10S)-3c-Hydroxy-10r.13c-dimethyl-17c-((1S:4R)-1.4.5-trimethyl-hexyl)-(5tH.8cH.9tH.14tH)-hexadecahydro-1H-cyclopenta[a]phenanthren

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (10S)-3c-Hydroxy-10r.13c-dimethyl-17c-((1S:4R)-1.4.5-trimethyl-hexyl)-(5tH.8cH.9tH.14tH)-hexadecahydro-1H-cyclopenta[a]phenanthren

There total 28 articles about (10S)-3c-Hydroxy-10r.13c-dimethyl-17c-((1S:4R)-1.4.5-trimethyl-hexyl)-(5tH.8cH.9tH.14tH)-hexadecahydro-1H-cyclopenta[a]phenanthren which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5β-lumistan-3β-ol (601-44-5) → 5β-lumistanol-(3α) (474-59-9,474-60-2,474-61-3,516-76-7,601-44-5,6538-02-9,17105-72-5,33947-18-1,35799-12-3,50298-91-4,58718-19-7,66036-55-3,70095-92-0,83861-56-7,96478-82-9,98463-66-2,103419-98-3,103419-99-4,106454-90-4,115458-67-8,115458-68-9,122087-74-5,122564-42-5,122564-43-6,122797-93-7,128050-56-6)

Guidance literature:

With ethanol; sodium ethanolate; at 200 ℃;

Reference yield:

5α,10α-ergostanol-(3β) (474-59-9) → 24βF-methyl-5α.10α-cholestanol-(3α) (474-59-9,474-60-2,474-61-3,516-76-7,601-44-5,6538-02-9,17105-72-5,33947-18-1,35799-12-3,50298-91-4,58718-19-7,66036-55-3,70095-92-0,83861-56-7,96478-82-9,98463-66-2,103419-98-3,103419-99-4,106454-90-4,115458-67-8,115458-68-9,122087-74-5,122564-42-5,122564-43-6,122797-93-7,128050-56-6)

Guidance literature:

With ethanol; sodium ethanolate; at 190 ℃;

DOI:10.1080/10473289.2002.10470843

Reference yield:

5α.10α-ergostadien-(7.22t)-yl-(3α)-acetate (1449-60-1,5035-34-7,27282-14-0,43085-34-3,50364-23-3,59042-24-9,59042-25-0,96646-07-0,115935-73-4,115935-81-4,137329-02-3) → 24βF-methyl-5α.10α-cholestanol-(3α) (474-59-9,474-60-2,474-61-3,516-76-7,601-44-5,6538-02-9,17105-72-5,33947-18-1,35799-12-3,50298-91-4,58718-19-7,66036-55-3,70095-92-0,83861-56-7,96478-82-9,98463-66-2,103419-98-3,103419-99-4,106454-90-4,115458-67-8,115458-68-9,122087-74-5,122564-42-5,122564-43-6,122797-93-7,128050-56-6)

Guidance literature:

With acetic acid; platinum; at 60 ℃; Hydrogenation_.Hydrolyse des gebildeten, nicht rein erhaltenen O-Acetyl-Derivats;

DOI:10.1080/10473289.2002.10470843

upstream raw materials:

(10S)-3c-Acetoxy-10r.13c-dimethyl-17c-((1R:4R)-1.4.5-trimethyl-hexen-(2t)-yl)-(5ξH.9cH.14tH)-Δ⁷-tetradecahydro-1H-cyclopenta[a]phenanthren

diethyl ether

acetic acid

(10R)-3c-Hydroxy-10r.13c-dimethyl-17c-((1R:4R)-1.4.5-trimethyl-hexen-(2t)-yl)-(9cH.14tH)-Δ^5.7-dodecahydro-1H-cyclopenta[a]phenanthren

Downstream raw materials:

O-Benzoyl-haliclonastanol