C₂₀H₁₇F₃O₃

Base Information

Chemical Name:C₂₀H₁₇F₃O₃
CAS No.:1453496-06-4
Molecular Formula:C₂₀H₁₇F₃O₃
Molecular Weight:362.348
Hs Code.:

C<sub>20</sub>H<sub>17</sub>F<sub>3</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₁₇F₃O₃

Chemical Property:

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Technology Process of C₂₀H₁₇F₃O₃

There total 7 articles about C₂₀H₁₇F₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 264279-00-7
4,4,4-trifluoro-1-(4-methoxyphenyl)-2-butyn-1-ol

: 1453496-06-4
C₂₀H₁₇F₃O₃

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 16 h / Reflux

2: triethylamine; (5aR,10bS)-5a,10b-dihydro-2-(2,4,6-trimethylphenyl)-4H,6H-indeno[2,1-b]-1,2,4-triazolo[4,3-d]-1,4-oxazinium chloride / dichloromethane-d2 / 20 °C

With (5aR,10bS)-5a,10b-dihydro-2-(2,4,6-trimethylphenyl)-4H,6H-indeno[2,1-b]-1,2,4-triazolo[4,3-d]-1,4-oxazinium chloride; triethylamine; In tetrahydrofuran; dichloromethane-d2;
DOI:10.1021/jo401433q

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1453496-06-4
C₂₀H₁₇F₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.08 h / -78 °C

1.2: 0.5 h / -78 °C

2.1: triethylamine / tetrahydrofuran / 16 h / Reflux

3.1: triethylamine; (5aR,10bS)-5a,10b-dihydro-2-(2,4,6-trimethylphenyl)-4H,6H-indeno[2,1-b]-1,2,4-triazolo[4,3-d]-1,4-oxazinium chloride / dichloromethane-d2 / 20 °C

With (5aR,10bS)-5a,10b-dihydro-2-(2,4,6-trimethylphenyl)-4H,6H-indeno[2,1-b]-1,2,4-triazolo[4,3-d]-1,4-oxazinium chloride; n-butyllithium; triethylamine; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane-d2;
DOI:10.1021/jo401433q

Reference yield:

: 17428-96-5
1,1-d2-3-phenylpropan-1-ol

: 1453496-06-4
C₂₀H₁₇F₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 3 h / 0 - 20 °C

2: tetra-(n-butyl)ammonium iodide; piperidine; tert.-butylhydroperoxide / decane; ethyl acetate / 5 h / 50 °C

3: triethylamine; (5aR,10bS)-5a,10b-dihydro-2-(2,4,6-trimethylphenyl)-4H,6H-indeno[2,1-b]-1,2,4-triazolo[4,3-d]-1,4-oxazinium chloride / dichloromethane-d2 / 20 °C

With piperidine; (5aR,10bS)-5a,10b-dihydro-2-(2,4,6-trimethylphenyl)-4H,6H-indeno[2,1-b]-1,2,4-triazolo[4,3-d]-1,4-oxazinium chloride; tert.-butylhydroperoxide; sulfur trioxide pyridine complex; tetra-(n-butyl)ammonium iodide; dimethyl sulfoxide; triethylamine; In decane; dichloromethane; dichloromethane-d2; ethyl acetate;
DOI:10.1021/jo401433q