[tricarbonylbis(triphenylphosphine)iridium] tetrafluoroborate

Base Information

Chemical Name:[tricarbonylbis(triphenylphosphine)iridium] tetrafluoroborate
CAS No.:52242-71-4
Molecular Formula:BF₄*C₃₉H₃₀IrO₃P₂
Molecular Weight:887.638
Hs Code.:

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Chemical Property of [tricarbonylbis(triphenylphosphine)iridium] tetrafluoroborate

Chemical Property:

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Technology Process of [tricarbonylbis(triphenylphosphine)iridium] tetrafluoroborate

There total 2 articles about [tricarbonylbis(triphenylphosphine)iridium] tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 328056-71-9
((C₈H₁₂)Ir((C₆H₅)2PCB₁₀H₁₀CCH₂N(CH₃)2))⁽¹⁺⁾*BF₄^(1-)=((C₈H₁₂)Ir((C₆H₅)2PCB₁₀H₁₀CCH₂N(CH₃)2))BF₄

: 201230-82-2
carbon monoxide

: 603-35-0
triphenylphosphine

: 52242-71-4,83111-60-8
[tricarbonylbis(triphenylphosphine)iridium] tetrafluoroborate

: 328056-67-3
o-C₂B₁₀H₁₀(CH₂NMe₂)(PPh₂)

Guidance literature:: In toluene; byproducts: COD; soln. iridium-carborane complex in toluene was treated with PPh3 at roomtemp. for 5 min, soln. was placed under atm. CO; volatile substances were removed in vacuo, residue was extd. with CH2Cl2, hexane was added; elem. anal.;
DOI:10.1016/S0022-328X(00)00607-0

Reference yield: 92.0%

: 83111-59-5
[dihydro(dicarbonyl)bis(triphenylphosphine)iridium] tetrafluoroborate

: 52242-71-4,83111-60-8
[tricarbonylbis(triphenylphosphine)iridium] tetrafluoroborate

Guidance literature:: With carbon monoxide; In benzene; CO bubbled through soln. of Ir complex in benzene for 2-3 h at 70-80°C; elem. anal.;
DOI:10.1016/S0022-328X(00)85705-8

Reference yield:

: 52242-71-4,83111-60-8
[tricarbonylbis(triphenylphosphine)iridium] tetrafluoroborate

: 143-66-8
sodium tetraphenyl borate

: 59809-88-0
[tricarbonylbis(triphenylphosphine)iridium] tetraphenylborate

Guidance literature:: In ethanol; soln. of Ir complex in ethanol treated with NaBPh4 in ethanol; elem. anal.; elem. anal.;
DOI:10.1016/S0022-328X(00)85705-8