C₅Me₄(SiMe₂N-2-C₆H₄Ph)TiI₂

Base Information

Chemical Name:C₅Me₄(SiMe₂N-2-C₆H₄Ph)TiI₂
CAS No.:1290103-51-3
Molecular Formula:C₂₃H₂₇I₂NSiTi
Molecular Weight:647.249
Hs Code.:

C<sub>5</sub>Me<sub>4</sub>(SiMe<sub>2</sub>N-2-C<sub>6</sub>H<sub>4</sub>Ph)TiI<sub>2</sub>

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Chemical Property of C₅Me₄(SiMe₂N-2-C₆H₄Ph)TiI₂

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Technology Process of C₅Me₄(SiMe₂N-2-C₆H₄Ph)TiI₂

There total 1 articles about C₅Me₄(SiMe₂N-2-C₆H₄Ph)TiI₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1290103-49-9
C₅Me₄(SiMe₂N-2-C₆H₄Ph)Ti(NMe₂)2

: 74-88-4
methyl iodide

: 1290103-51-3
C₅Me₄(SiMe₂N-2-C₆H₄Ph)TiI₂

Guidance literature:: In dichloromethane; (N2) to soln. Ti complex in CH2Cl2 MeI was added, stirred for 12 h; soln. was filtered through Celite, solvent was removed in vacuo, residuewas washed with cold pentane; elem. anal.;
DOI:10.1039/c0dt01530j

Reference yield: 82.0%

: 1290103-51-3
C₅Me₄(SiMe₂N-2-C₆H₄Ph)TiI₂

: 75-16-1
methylmagnesium bromide

: 1290103-54-6
C₅Me₄(SiMe₂N-2-C₆H₄Ph)TiMe₂

Guidance literature:: In tetrahydrofuran; diethyl ether; (N2) to soln. Ti complex in THF at -35°C soln. MeMgBr in Et2O wasadded; solvent was removed in vacuo, residue was extd. with pentane and filtered through Celite, soln. was evapd. in vacuo; elem. anal.;
DOI:10.1039/c0dt01530j