C₂₉H₃₁F₉N₈O₂

Base Information

Chemical Name:C₂₉H₃₁F₉N₈O₂
CAS No.:867012-02-0
Molecular Formula:C₂₉H₃₁F₉N₈O₂
Molecular Weight:694.603
Hs Code.:

C<sub>29</sub>H<sub>31</sub>F<sub>9</sub>N<sub>8</sub>O<sub>2</sub>

Synonyms:

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Chemical Property of C₂₉H₃₁F₉N₈O₂

Chemical Property:

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Technology Process of C₂₉H₃₁F₉N₈O₂

There total 8 articles about C₂₉H₃₁F₉N₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-52-5
N-methyl-4-hydroxypiperidine

: 867012-73-5
C₂₃H₁₉ClF₉N₇O

: 867012-02-0
C₂₉H₃₁F₉N₈O₂

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1016/j.bmcl.2012.03.075

Reference yield:

: C₂₄H₂₄F₉N₃O₂

: 867012-02-0
C₂₉H₃₁F₉N₈O₂

Guidance literature:: Multi-step reaction with 7 steps

1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

2: sodium azide; triethylamine / toluene / 110 °C

3: potassium carbonate / acetonitrile

4: Chiralpak AD / Resolution of racemate

5: sulfuric acid; trifluoroacetic acid / 0 - 20 °C

6: triethylamine / toluene

7: dmap / dichloromethane / 20 h / 20 °C

With dmap; sodium azide; sulfuric acid; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.075

Reference yield:

: C₁₇H₂₂F₃N₃O₃

: 867012-02-0
C₂₉H₃₁F₉N₈O₂

Guidance literature:: Multi-step reaction with 9 steps

1: hydrogenchloride / water / 80 °C

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

4: sodium azide; triethylamine / toluene / 110 °C

5: potassium carbonate / acetonitrile

6: Chiralpak AD / Resolution of racemate

7: sulfuric acid; trifluoroacetic acid / 0 - 20 °C

8: triethylamine / toluene

9: dmap / dichloromethane / 20 h / 20 °C

With hydrogenchloride; dmap; sodium azide; sulfuric acid; sodium tris(acetoxy)borohydride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2012.03.075