2,4,8,10-tetrakis-(1-methyl-1-phenyl-ethyl)-6-(2,2,2-trifluoro-ethoxy)-5,7-dioxa-12-thia-6-phospha-dibenzo[a,d]cyclooctene 12,12-dioxide

Base Information

• Chemical Name: 2,4,8,10-tetrakis-(1-methyl-1-phenyl-ethyl)-6-(2,2,2-trifluoro-ethoxy)-5,7-dioxa-12-thia-6-phospha-dibenzo[a,d]cyclooctene 12,12-dioxide
• CAS No.: 921201-42-5
• Molecular Formula: C₅₀H₅₀F₃O₅PS
• Molecular Weight: 850.979
• Mol file: 921201-42-5.mol

Synonyms:

Chemical Property of 2,4,8,10-tetrakis-(1-methyl-1-phenyl-ethyl)-6-(2,2,2-trifluoro-ethoxy)-5,7-dioxa-12-thia-6-phospha-dibenzo[a,d]cyclooctene 12,12-dioxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,8,10-tetrakis-(1-methyl-1-phenyl-ethyl)-6-(2,2,2-trifluoro-ethoxy)-5,7-dioxa-12-thia-6-phospha-dibenzo[a,d]cyclooctene 12,12-dioxide

There total 3 articles about 2,4,8,10-tetrakis-(1-methyl-1-phenyl-ethyl)-6-(2,2,2-trifluoro-ethoxy)-5,7-dioxa-12-thia-6-phospha-dibenzo[a,d]cyclooctene 12,12-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C48H50O4S (918424-28-9) → 2,4,8,10-tetrakis-(1-methyl-1-phenyl-ethyl)-6-(2,2,2-trifluoro-ethoxy)-5,7-dioxa-12-thia-6-phospha-dibenzo[a,d]cyclooctene 12,12-dioxide (921201-42-5)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus trichloride; triethylamine / CH₂Cl₂ / 2 h

2: CH₂Cl₂ / 24 h

With triethylamine; phosphorus trichloride; In dichloromethane;

DOI:10.1080/10426500600683126

Reference yield:

2,4-di-cumylphenol (2772-45-4,106060-52-0) → 2,4,8,10-tetrakis-(1-methyl-1-phenyl-ethyl)-6-(2,2,2-trifluoro-ethoxy)-5,7-dioxa-12-thia-6-phospha-dibenzo[a,d]cyclooctene 12,12-dioxide (921201-42-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sulfur dichloride; zinc chloride / hexane / 48 h

1.2: 22 percent / acetic acid; aq. hydrogen peroxide / 2 h / Heating

2.1: phosphorus trichloride; triethylamine / CH₂Cl₂ / 2 h

3.1: CH₂Cl₂ / 24 h

With sulfur dichloride; triethylamine; zinc(II) chloride; phosphorus trichloride; In hexane; dichloromethane;

DOI:10.1080/10426500600683126

Reference yield:

6-chloro-2,4,8,10-tetrakis-(1-methyl-1-phenyl-ethyl)-5,7-dioxa-12-thia-6-phospha-dibenzo[a,d]cyclooctene 12,12-dioxide + 2,2,2-trifluoroethanol (75-89-8) → 2,4,8,10-tetrakis-(1-methyl-1-phenyl-ethyl)-6-(2,2,2-trifluoro-ethoxy)-5,7-dioxa-12-thia-6-phospha-dibenzo[a,d]cyclooctene 12,12-dioxide (921201-42-5)

Guidance literature:

In dichloromethane; for 24h;

DOI:10.1080/10426500600683126

upstream raw materials:

2,2,2-trifluoroethanol

C₄₈H₅₀O₄S

2,4-di-cumylphenol