Technology Process of 7-oximino-1-phenyl-trans-bicyclo<4.3.0>nonan-8-one
There total 4 articles about 7-oximino-1-phenyl-trans-bicyclo<4.3.0>nonan-8-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 53 percent / zinc / diethyl ether; benzene / 3 h / Heating
2: 1.) anhydrous aluminium chloride; 2.) potassium hydroxide / 1.) benzene, 5 deg C then rt. overnight; 2.) ethanol, reflux, 4h
3: 74 percent / sodium acetate, methanol / acetic anhydride / 2.5 h / Heating
4: 22 percent / hydrogen chloride(gas), n-butyl nitrite / diethyl ether / Heating
With
hydrogenchloride; methanol; potassium hydroxide; aluminium trichloride; n-Butyl nitrite; sodium acetate; zinc;
In
diethyl ether; acetic anhydride; benzene;
DOI:10.1016/S0040-4020(01)85936-6
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) anhydrous aluminium chloride; 2.) potassium hydroxide / 1.) benzene, 5 deg C then rt. overnight; 2.) ethanol, reflux, 4h
2: 74 percent / sodium acetate, methanol / acetic anhydride / 2.5 h / Heating
3: 22 percent / hydrogen chloride(gas), n-butyl nitrite / diethyl ether / Heating
With
hydrogenchloride; methanol; potassium hydroxide; aluminium trichloride; n-Butyl nitrite; sodium acetate;
In
diethyl ether; acetic anhydride;
DOI:10.1016/S0040-4020(01)85936-6
