1,3,5-tris(ethylsulfinyl)-2,4,6-trimethylbenznene

Base Information

• Chemical Name: 1,3,5-tris(ethylsulfinyl)-2,4,6-trimethylbenznene
• CAS No.: 776296-64-1
• Molecular Formula: C₁₈H₃₀O₃S₃
• Molecular Weight: 390.632

Synonyms:

Chemical Property of 1,3,5-tris(ethylsulfinyl)-2,4,6-trimethylbenznene

Chemical Property:

Purity/Quality:

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Technology Process of 1,3,5-tris(ethylsulfinyl)-2,4,6-trimethylbenznene

There total 1 articles about 1,3,5-tris(ethylsulfinyl)-2,4,6-trimethylbenznene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

1,3,5-tris-ethylsulfanylmethyl-2,4,6-trimethyl-benzene → 1,3,5-tris(ethylsulfinyl)-2,4,6-trimethylbenznene (776296-64-1)

Guidance literature:

With nitric acid; In benzene; for 24h;

DOI:10.1002/ejic.200300751

Reference yield: 39.0%

methanol (67-56-1) + lanthanum(III) nitrate hydrated + 1,3,5-tris(ethylsulfinyl)-2,4,6-trimethylbenznene (776296-64-1) → [(1,3,5-tris(ethylsulfinyl)-2,4,6-trimethylbenznene)(methanol)trinitratolanthanum(III)]n

Guidance literature:

With triethyl orthoformate; In methanol; chloroform; triethyl orthoformate added to a soln. of ligand (CHCl3), stirred for 20min, a soln. of metal salt (methanol) added, stirred at 70-80°C for ca. 4 h; cooled to room temp., filtered, allowed to stand at room temp. for 1 wk;elem. anal.;

DOI:10.1002/ejic.200300751

Reference yield: 34.0%

methanol (67-56-1) + neodymium(III) nitrate hydrate + 1,3,5-tris(ethylsulfinyl)-2,4,6-trimethylbenznene (776296-64-1) → [(1,3,5-tris(ethylsulfinyl)-2,4,6-trimethylbenznene)(methanol)trinitratoneodymium(III)]n

Guidance literature:

With triethyl orthoformate; In methanol; chloroform; triethyl orthoformate added to a soln. of ligand (CHCl3), stirred for 20min, a soln. of metal salt (methanol) added, stirred at 70-80°C for ca. 4 h; cooled to room temp., filtered, allowed to stand at room temp. for 1 wk;elem. anal.;

DOI:10.1002/ejic.200300751

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