Ni((N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)(MeCN)Cl(ClO₄)

Base Information

• Chemical Name: Ni((N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)(MeCN)Cl(ClO₄)
• CAS No.: 727994-38-9
• Molecular Formula: C₃₂H₂₉ClN₅Ni*ClO₄
• Molecular Weight: 677.209

Synonyms:

Chemical Property of Ni((N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)(MeCN)Cl(ClO₄)

Chemical Property:

Purity/Quality:

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Technology Process of Ni((N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)(MeCN)Cl(ClO₄)

There total 1 articles about Ni((N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)(MeCN)Cl(ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

nickel(II) perchlorate hexahydrate + N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)-methyl)amine (167897-42-9) + tetramethlyammonium chloride (75-57-0) + acetonitrile (75-05-8,26809-02-9) → Ni((N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)(MeCN)Cl(ClO4) (727994-38-9)

Guidance literature:

In acetonitrile; MeCN soln. of ligand was added to MeCN soln. of Ni(ClO4)2*6H2O, stirred for 1 h, Me4NCl in MeCN was added, stirred for 1 h; solvent was removed under reduced pressure, redissolved in CH2Cl2, filtered, evapd. to dryness, recrystd. from MeCN/Et2O at ambient temp.; elem.anal.;

DOI:10.1021/ic040002a

upstream raw materials:

N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)-methyl)amine

tetramethlyammonium chloride

acetonitrile

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